Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7718763
Preview
| Coordinates | 7718763.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C17 H25 B N4 O6 |
|---|---|
| Calculated formula | C17 H25 B N4 O6 |
| Title of publication | Transition metal(IV) complexes of nitro-substituted 2,4,9-triazaadamantane-based tris-hydroxylamines: evidence for nitrogen α-effect on stabilization of higher oxidation states. |
| Authors of publication | Pospelov, Evgeny V.; Sinyushin, Kirill I.; Golovanov, Ivan S.; Lesnikov, Vladislav K.; Frolov, Kirill V.; Nelyubina, Yulia V.; Sukhorukov, Alexey Yu |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2025 |
| Journal volume | 54 |
| Journal issue | 24 |
| Pages of publication | 9530 - 9541 |
| a | 10.25318 ± 0.00006 Å |
| b | 10.89893 ± 0.00007 Å |
| c | 16.74915 ± 0.00012 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1871.7 ± 0.02 Å3 |
| Cell temperature | 100 ± 0.1 K |
| Ambient diffraction temperature | 100 ± 0.1 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0308 |
| Residual factor for significantly intense reflections | 0.0305 |
| Weighted residual factors for significantly intense reflections | 0.081 |
| Weighted residual factors for all reflections included in the refinement | 0.0814 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.073 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 300748 (current) | 2025-07-06 | cif/ Updating files of 7718760, 7718761, 7718762, 7718763, 7718764, 7718765 Original log message: Adding full bibliography for 7718760--7718765.cif. |
7718763.cif |
| 299752 | 2025-05-21 | cif/ Adding structures of 7718760, 7718761, 7718762, 7718763, 7718764, 7718765 via cif-deposit CGI script. |
7718763.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.