#------------------------------------------------------------------------------ #$Date: 2025-05-22 01:52:18 +0300 (Thu, 22 May 2025) $ #$Revision: 299776 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/71/87/7718778.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7718778 loop_ _publ_author_name 'Jangra, Reena' 'Nair, Amritha J.' 'Kuriakose, Albin' 'Acharyya, Jitendra Nath' 'Prakash, Gaddam Vijaya' 'Sankar, Muniappan' _publ_section_title ; Electron Deficient \b-Trisubstituted Porphyrins: Synthesis, Structural, Spectral, and Electrochemical Studies and Their Intensity-Dependent Third-Order Nonlinear Optical Studies ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D5DT00618J _journal_year 2025 _chemical_formula_moiety 'C46 H25 Co F6 N5 O2, C H Cl3' _chemical_formula_sum 'C47 H26 Cl3 Co F6 N5 O2' _chemical_formula_weight 972.01 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-05-21 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2024-10-07 deposited with the CCDC. 2025-05-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 103.4240(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.1880(4) _cell_length_b 25.7080(8) _cell_length_c 12.8575(4) _cell_measurement_reflns_used 9894 _cell_measurement_temperature 100.00 _cell_measurement_theta_max 23.276 _cell_measurement_theta_min 2.221 _cell_volume 3918.6(2) _computing_cell_refinement 'SAINT V8.40B (Bruker AXS LLC, 2019)' _computing_data_collection 'Bruker APEX4 v2022.1-0 (Bruker AXS Inc., 2022)' _computing_data_reduction 'SAINT V8.40B (Bruker AXS LLC, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 100.00 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker D8 QUEST Photon III C7' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1044 _diffrn_reflns_av_unetI/netI 0.0475 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 30 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 118855 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.208 _diffrn_reflns_theta_max 25.208 _diffrn_reflns_theta_min 1.584 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 0.722 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.7070 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1383 before and 0.0767 after correction. The Ratio of minimum to maximum transmission is 0.9487. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'metallic dark blue' _exptl_crystal_density_diffrn 1.648 _exptl_crystal_description block _exptl_crystal_F_000 1964 _exptl_crystal_size_max 0.174 _exptl_crystal_size_mid 0.118 _exptl_crystal_size_min 0.098 _refine_diff_density_max 0.796 _refine_diff_density_min -0.573 _refine_diff_density_rms 0.098 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.021 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 604 _refine_ls_number_reflns 7045 _refine_ls_number_restraints 18 _refine_ls_restrained_S_all 1.025 _refine_ls_R_factor_all 0.0761 _refine_ls_R_factor_gt 0.0506 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0599P)^2^+8.8398P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1208 _refine_ls_wR_factor_ref 0.1370 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5286 _reflns_number_total 7045 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d5dt00618j2.cif _cod_data_source_block ms_rj_cono2_cf3_2_1035_0m _cod_database_code 7718778 _shelx_shelxl_version_number 2019/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2. Uiso/Uaniso restraints and constraints Uanis(F1) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(F8) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(F7) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 3. Others Fixed Sof: F1(0.4) F7(0.6) F8(0.6) F3(0.4) F2(0.4) F9(0.6) 4.a Ternary CH refined with riding coordinates: C47(H47) 4.b Aromatic/amide H refined with riding coordinates: C3(H3), C8(H8), C25(H25), C26(H26), C7(H7), C28(H28), C23(H23), C38(H38), C43(H43), C18(H18), C40(H40), C41(H41), C24(H24), C37(H37), C17(H17), C36(H36), C44(H44), C29(H29), C22(H22), C42(H42), C31(H31), C32(H32), C35(H35), C30(H30), C34(H34) ; _shelx_res_file ; TITL ms_rj_cono2_cf3_2_1035_0m_a.res in P2(1)/c ms_rj_cono2_cf3_2_1035_0m.res created by SHELXL-2019/1 at 15:45:23 on 21-May-2024 REM Old TITL MS_RJ_CoNO2_CF3_2_1035_0m in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.146, Rweak 0.008, Alpha 0.042 REM 0.422 for 186 systematic absences, Orientation as input REM Formula found by SHELXT: C53 Cl3 Co F8 N3 O3 CELL 0.71073 12.188 25.708 12.8575 90 103.424 90 ZERR 4 0.0004 0.0008 0.0004 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cl Co F N O UNIT 188 104 12 4 24 20 8 ISOR 0.001 0.002 F1 ISOR 0.001 0.002 F8 ISOR 0.001 0.002 F7 L.S. 4 PLAN 1 TEMP -173.15 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta OMIT 0 0 4 REM REM REM WGHT 0.059900 8.839800 FVAR 0.32701 CO1 4 0.485198 0.631152 0.466535 11.00000 0.01138 0.02428 = 0.01845 -0.00421 0.00076 0.00084 CL2 3 -0.158583 0.499483 -0.038155 11.00000 0.03147 0.04300 = 0.03954 -0.00451 0.00645 -0.00463 CL1 3 -0.319882 0.484123 0.092002 11.00000 0.03391 0.06027 = 0.04557 -0.01001 0.01152 0.00612 CL3 3 -0.140770 0.410461 0.103469 11.00000 0.04895 0.05154 = 0.05175 0.00443 0.00245 0.01366 F6 5 0.684788 0.792933 0.842023 11.00000 0.04628 0.03776 = 0.04139 -0.02037 0.02241 -0.02119 F5 5 0.513925 0.766014 0.809256 11.00000 0.02252 0.06349 = 0.02488 -0.00898 0.00694 0.00915 F4 5 0.644343 0.721425 0.906651 11.00000 0.05761 0.03626 = 0.01995 0.00033 0.00529 0.00579 N3 6 0.587444 0.675955 0.565845 11.00000 0.01372 0.02293 = 0.01820 -0.00143 0.00133 0.00087 N4 6 0.365259 0.681698 0.456791 11.00000 0.01302 0.02550 = 0.01914 -0.00199 0.00148 -0.00101 O2 7 0.064324 0.486428 0.250235 11.00000 0.02956 0.03752 = 0.04601 -0.00328 0.00137 -0.00878 N2 6 0.609703 0.586071 0.457290 11.00000 0.01370 0.02636 = 0.01807 -0.00300 0.00053 -0.00130 O1 7 0.041803 0.540877 0.372954 11.00000 0.02831 0.04946 = 0.05637 -0.00083 0.02192 0.00101 N1 6 0.379690 0.581524 0.387180 11.00000 0.01527 0.02487 = 0.02121 -0.00353 0.00124 0.00222 N00E 6 0.098592 0.520450 0.317083 11.00000 0.02353 0.03338 = 0.03363 0.00071 0.00380 -0.00111 C14 1 0.553922 0.715542 0.623703 11.00000 0.01477 0.02291 = 0.01800 0.00026 0.00331 -0.00309 C16 1 0.380088 0.733034 0.490974 11.00000 0.01477 0.02296 = 0.01882 -0.00206 0.00397 -0.00005 C11 1 0.697852 0.664766 0.614400 11.00000 0.01465 0.02599 = 0.01922 0.00054 0.00067 0.00028 C9 1 0.722215 0.601448 0.481307 11.00000 0.01490 0.02782 = 0.01726 0.00254 0.00118 0.00284 C3 1 0.299310 0.501266 0.335862 11.00000 0.01934 0.02406 = 0.02448 -0.00323 0.00567 -0.00161 AFIX 43 H3 2 0.291532 0.465113 0.320633 11.00000 -1.20000 AFIX 0 C8 1 0.785250 0.569031 0.424311 11.00000 0.01512 0.02992 = 0.02414 -0.00084 0.00349 0.00329 AFIX 43 H8 2 0.862079 0.573202 0.421944 11.00000 -1.20000 AFIX 0 C13 1 0.637318 0.722178 0.722122 11.00000 0.01890 0.02294 = 0.02104 -0.00091 0.00408 -0.00236 C46 1 0.619955 0.750598 0.818871 11.00000 0.01728 0.02586 = 0.02439 -0.00307 0.00261 -0.00380 C4 1 0.402355 0.530167 0.366454 11.00000 0.01458 0.02459 = 0.01854 -0.00052 0.00262 0.00011 C6 1 0.605288 0.541825 0.396397 11.00000 0.01922 0.02597 = 0.01582 -0.00130 0.00098 0.00267 C25 1 -0.028936 0.621772 0.097503 11.00000 0.01989 0.03412 = 0.02816 -0.00823 -0.00045 0.00229 AFIX 43 H25 2 -0.039102 0.609129 0.026474 11.00000 -1.20000 AFIX 0 C15 1 0.464299 0.749078 0.576503 11.00000 0.01768 0.02460 = 0.01848 -0.00119 0.00572 -0.00375 C12 1 0.727534 0.691211 0.715230 11.00000 0.01728 0.02885 = 0.02001 -0.00193 0.00029 -0.00381 C21 1 0.092886 0.637582 0.271310 11.00000 0.01505 0.02528 = 0.02738 -0.00552 0.00059 0.00168 C26 1 0.075993 0.618759 0.167646 11.00000 0.01592 0.03085 = 0.02961 -0.00857 0.00418 0.00244 AFIX 43 H26 2 0.137272 0.603586 0.144438 11.00000 -1.20000 AFIX 0 C7 1 0.714226 0.531716 0.375102 11.00000 0.01972 0.02466 = 0.02258 -0.00220 0.00459 0.00373 AFIX 43 H7 2 0.732668 0.503798 0.333838 11.00000 -1.20000 AFIX 0 C2 1 0.216147 0.535751 0.333158 11.00000 0.01469 0.03402 = 0.02394 -0.00636 0.00250 -0.00147 C28 1 0.445756 0.451624 0.205781 11.00000 0.02116 0.02649 = 0.03035 -0.00216 0.00610 0.00139 AFIX 43 H28 2 0.389633 0.476401 0.175335 11.00000 -1.20000 AFIX 0 C10 1 0.767731 0.637591 0.559541 11.00000 0.01633 0.02760 = 0.01836 -0.00091 -0.00167 0.00221 C39 1 0.472877 0.805050 0.606883 11.00000 0.02099 0.02400 = 0.02057 -0.00160 0.00462 -0.00081 C1 1 0.263404 0.586814 0.359382 11.00000 0.01258 0.03066 = 0.02172 -0.00732 0.00129 -0.00107 C27 1 0.516942 0.461587 0.305565 11.00000 0.01881 0.02261 = 0.02434 0.00012 0.00661 -0.00089 C23 1 -0.103548 0.661592 0.234165 11.00000 0.01413 0.03993 = 0.03632 -0.00221 0.00305 0.00575 AFIX 43 H23 2 -0.165631 0.676045 0.257210 11.00000 -1.20000 AFIX 0 C38 1 0.910779 0.706682 0.566826 11.00000 0.01825 0.02682 = 0.02517 -0.00098 0.00111 0.00394 AFIX 43 H38 2 0.850291 0.730911 0.552142 11.00000 -1.20000 AFIX 0 C19 1 0.262443 0.680395 0.384140 11.00000 0.01136 0.02951 = 0.02212 -0.00400 0.00209 0.00139 C43 1 0.393677 0.887223 0.643304 11.00000 0.02332 0.03182 = 0.02853 -0.00523 0.00264 0.00619 AFIX 43 H43 2 0.331129 0.907050 0.653241 11.00000 -1.20000 AFIX 0 C18 1 0.217873 0.732136 0.365311 11.00000 0.01746 0.03250 = 0.02138 -0.00033 0.00038 0.00353 AFIX 43 H18 2 0.149979 0.741862 0.316275 11.00000 -1.20000 AFIX 0 C40 1 0.575363 0.830104 0.612282 11.00000 0.02047 0.02544 = 0.02121 -0.00164 0.00421 -0.00123 AFIX 43 H40 2 0.638159 0.810795 0.601275 11.00000 -1.20000 AFIX 0 C41 1 0.586624 0.882952 0.633565 11.00000 0.02408 0.02552 = 0.02585 0.00125 0.00287 -0.00256 AFIX 43 H41 2 0.657350 0.899558 0.638916 11.00000 -1.20000 AFIX 0 C24 1 -0.118611 0.643181 0.131076 11.00000 0.01522 0.03625 = 0.03282 -0.00110 -0.00288 0.00294 AFIX 43 H24 2 -0.190701 0.645239 0.083208 11.00000 -1.20000 AFIX 0 C5 1 0.508632 0.511766 0.361184 11.00000 0.01999 0.02697 = 0.01617 0.00184 0.00335 0.00211 C37 1 1.020686 0.724397 0.579356 11.00000 0.02286 0.02447 = 0.03009 -0.00059 0.00116 -0.00258 AFIX 43 H37 2 1.034976 0.760485 0.573605 11.00000 -1.20000 AFIX 0 C33 1 0.887641 0.653955 0.575420 11.00000 0.01505 0.02858 = 0.02022 -0.00477 0.00080 0.00080 C17 1 0.289897 0.764190 0.429813 11.00000 0.01701 0.02439 = 0.02384 -0.00072 0.00352 -0.00014 AFIX 43 H17 2 0.282620 0.800866 0.434275 11.00000 -1.20000 AFIX 0 C45 1 0.828107 0.679817 0.804245 11.00000 0.02605 0.03554 = 0.02378 -0.00965 -0.00270 0.00748 C36 1 1.109270 0.689461 0.600204 11.00000 0.01542 0.03452 = 0.03133 0.00139 0.00233 -0.00297 AFIX 43 H36 2 1.184512 0.701520 0.608704 11.00000 -1.20000 AFIX 0 C44 1 0.381993 0.834003 0.625188 11.00000 0.01747 0.03162 = 0.02500 -0.00229 0.00429 0.00051 AFIX 43 H44 2 0.312456 0.817317 0.625233 11.00000 -1.20000 AFIX 0 C20 1 0.208208 0.634636 0.343544 11.00000 0.01253 0.03176 = 0.02211 -0.00657 0.00141 0.00119 C29 1 0.455343 0.406295 0.150245 11.00000 0.02767 0.03403 = 0.03283 -0.00757 0.00668 -0.00811 AFIX 43 H29 2 0.406213 0.400443 0.082246 11.00000 -1.20000 AFIX 0 C22 1 0.002067 0.659160 0.304826 11.00000 0.01850 0.03229 = 0.02841 -0.00952 0.00357 0.00077 AFIX 43 H22 2 0.012062 0.672170 0.375565 11.00000 -1.20000 AFIX 0 C42 1 0.494958 0.911335 0.646940 11.00000 0.03083 0.02459 = 0.02684 -0.00350 0.00281 0.00164 AFIX 43 H42 2 0.501919 0.947789 0.658739 11.00000 -1.20000 AFIX 0 C31 1 0.605089 0.378302 0.292148 11.00000 0.02326 0.02023 = 0.05569 0.00907 0.01798 0.00360 AFIX 43 H31 2 0.659178 0.352740 0.323025 11.00000 -1.20000 AFIX 0 C32 1 0.597103 0.424305 0.348216 11.00000 0.01754 0.03215 = 0.02814 0.00670 0.00548 -0.00178 AFIX 43 H32 2 0.646907 0.430031 0.415917 11.00000 -1.20000 AFIX 0 C35 1 1.088333 0.636832 0.608712 11.00000 0.01629 0.03085 = 0.04039 0.00423 0.00189 0.00458 AFIX 43 H35 2 1.149321 0.612866 0.623042 11.00000 -1.20000 AFIX 0 C30 1 0.535698 0.369650 0.193037 11.00000 0.03104 0.02642 = 0.04702 -0.00988 0.01604 -0.00880 AFIX 43 H30 2 0.543022 0.338807 0.154515 11.00000 -1.20000 AFIX 0 C34 1 0.978284 0.618980 0.596333 11.00000 0.01782 0.02576 = 0.04137 0.00068 0.00249 -0.00217 AFIX 43 H34 2 0.964510 0.582843 0.602097 11.00000 -1.20000 AFIX 0 C47 1 -0.178050 0.476591 0.085587 11.00000 0.03552 0.05209 = 0.03394 -0.00737 0.00190 0.00246 AFIX 13 H47 2 -0.129238 0.497269 0.144435 11.00000 -1.20000 AFIX 0 PART 2 F1 5 0.865194 0.632689 0.799248 10.40000 0.02994 0.02995 = 0.03161 0.00030 0.00333 0.00268 PART 1 F7 5 0.864924 0.719216 0.862967 10.60000 0.04075 0.04646 = 0.04096 -0.00525 0.00076 -0.00149 F8 5 0.789832 0.644732 0.875143 10.60000 0.04250 0.05001 = 0.04353 0.00591 0.00606 0.00048 PART 2 F3 5 0.920319 0.712854 0.791992 10.40000 0.01514 0.03865 = 0.02832 -0.00116 -0.01363 -0.01009 F2 5 0.820330 0.690441 0.899425 10.40000 0.03320 0.05011 = 0.00967 -0.00161 -0.00295 0.02040 PART 1 F9 5 0.909189 0.652510 0.782045 10.60000 0.03017 0.08936 = 0.02197 -0.00605 -0.00524 0.03127 HKLF 4 REM ms_rj_cono2_cf3_2_1035_0m_a.res in P2(1)/c REM wR2 = 0.1370, GooF = S = 1.021, Restrained GooF = 1.025 for all data REM R1 = 0.0506 for 5286 Fo > 4sig(Fo) and 0.0761 for all 7045 data REM 604 parameters refined using 18 restraints END WGHT 0.0599 8.8400 REM Highest difference peak 0.796, deepest hole -0.573, 1-sigma level 0.098 Q1 1 0.3316 0.4243 0.3359 11.00000 0.05 0.80 ; _shelx_res_checksum 67365 _shelx_hkl_file ; 1 0 0 5181.78 243.58 -2 0 0 2761.82 115.79 -2 0 0 2693.93 120.49 -2 0 0 2735.23 117.29 -2 0 0 2598.74 112.69 2 0 0 2779.92 120.39 2 0 0 2605.54 115.29 2 0 0 2721.73 120.49 2 0 0 2709.53 117.19 2 0 0 2723.33 113.19 -2 0 0 2589.74 120.29 2 0 0 2710.33 112.69 3 0 0 1852.81 88.49 3 0 0 1850.41 77.39 -3 0 0 1712.03 88.69 3 0 0 1801.22 83.59 3 0 0 1858.01 78.39 -3 0 0 1775.52 81.59 -3 0 0 1689.03 87.79 -3 0 0 1775.32 83.89 -3 0 0 1765.82 77.39 3 0 0 1795.42 81.49 3 0 0 1797.62 88.29 4 0 0 780.02 42.30 4 0 0 794.12 50.19 4 0 0 745.93 44.30 -4 0 0 794.42 37.70 -4 0 0 764.72 51.19 -4 0 0 792.32 42.70 -4 0 0 863.11 51.89 -4 0 0 811.92 45.70 4 0 0 765.42 37.10 4 0 0 833.72 51.29 4 0 0 739.63 38.60 5 0 0 1574.04 70.89 -5 0 0 1657.83 84.39 -5 0 0 1577.94 82.49 -5 0 0 1578.54 71.79 -5 0 0 1491.95 88.09 5 0 0 1596.94 88.39 5 0 0 1562.14 77.99 5 0 0 1631.74 88.99 5 0 0 1502.75 80.79 -5 0 0 1688.13 79.69 -5 0 0 1588.14 98.39 5 0 0 1640.94 73.99 6 0 0 364.26 42.40 -6 0 0 313.17 26.60 -6 0 0 327.27 34.80 6 0 0 374.96 41.40 6 0 0 290.97 18.60 -6 0 0 275.37 37.90 -6 0 0 274.17 37.00 -6 0 0 256.07 31.10 6 0 0 264.77 30.30 6 0 0 309.97 22.50 -6 0 0 332.17 20.20 -7 0 0 292.17 30.70 -7 0 0 267.57 40.30 7 0 0 238.98 37.40 7 0 0 254.37 31.90 -7 0 0 273.67 34.20 7 0 0 267.57 38.30 -7 0 0 254.47 18.30 7 0 0 244.88 21.00 -7 0 0 281.57 33.90 -7 0 0 261.17 46.10 7 0 0 222.78 16.10 -8 0 0 1013.80 61.49 8 0 0 1024.70 46.20 -8 0 0 1040.80 50.59 8 0 0 1073.99 74.39 -8 0 0 865.41 73.49 -8 0 0 1040.50 76.09 8 0 0 1001.20 54.19 8 0 0 955.10 72.89 8 0 0 889.21 62.69 -8 0 0 950.60 65.89 -8 0 0 889.81 65.99 -9 0 0 822.82 71.79 -9 0 0 747.83 52.89 -9 0 0 738.93 65.59 -9 0 0 704.13 56.49 -9 0 0 753.32 59.79 -9 0 0 725.83 40.70 9 0 0 742.23 45.30 -10 0 0 1151.18 71.09 -10 0 0 1065.59 77.29 -10 0 0 1010.90 109.69 -10 0 0 1078.19 91.99 -10 0 0 1016.50 75.69 -10 0 0 1087.69 86.99 -10 0 0 1085.99 55.99 10 0 0 1167.88 62.39 -10 0 0 1090.99 75.89 11 0 0 77.29 16.70 -11 0 0 93.19 22.20 -11 0 0 96.99 13.90 -11 0 0 78.89 24.90 -11 0 0 93.89 31.20 -12 0 0 5.70 15.40 -12 0 0 -6.00 4.50 -12 0 0 10.60 14.40 12 0 0 -3.20 8.30 -12 0 0 0.10 10.80 -13 0 0 79.49 32.70 13 0 0 84.59 18.60 -13 0 0 90.89 13.10 -13 0 0 80.09 25.80 -14 0 0 -19.40 10.90 -14 0 0 -0.60 18.00 14 0 0 -3.80 9.10 -1 -1 0 767.32 32.70 1 -1 0 719.63 34.70 -1 -1 0 716.43 34.40 1 -1 0 753.22 36.50 1 -1 0 743.03 32.50 -1 -1 0 732.83 35.10 -1 -1 0 756.72 36.70 1 1 0 736.73 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9.90 7.90 -2 3 0 2.10 8.70 -3 -3 0 1892.61 93.99 3 -3 0 1867.71 85.49 -3 -3 0 1936.01 86.29 -3 -3 0 1947.51 108.29 3 -3 0 1937.71 86.19 3 -3 0 1947.81 85.69 3 -3 0 1955.50 91.49 3 -3 0 1871.81 96.49 -3 -3 0 1966.60 98.19 -3 -3 0 1921.51 93.79 -3 -3 0 1857.41 91.29 3 3 0 1993.10 88.79 -3 3 0 1939.41 86.09 -3 3 0 1793.92 95.09 -3 3 0 1976.70 86.29 -3 3 0 1900.81 85.19 -3 3 0 1943.11 84.09 -3 3 0 1954.60 85.09 -3 3 0 2033.80 87.69 -3 3 0 1987.30 92.19 3 3 0 1893.71 97.19 3 3 0 1924.41 85.59 -3 3 0 1874.01 96.19 3 3 0 2033.10 94.69 3 3 0 1975.10 93.39 -3 3 0 2021.40 91.79 3 3 0 1907.61 91.29 -4 -3 0 2.60 13.60 -4 -3 0 4.00 8.60 4 -3 0 4.60 5.20 -4 -3 0 3.40 4.70 -4 -3 0 -1.30 6.80 -4 -3 0 12.70 8.40 4 -3 0 9.50 7.70 -4 -3 0 7.00 7.20 4 -3 0 4.60 4.70 4 -3 0 9.00 4.70 -4 3 0 14.80 6.00 -4 3 0 12.20 5.90 4 3 0 -0.50 6.70 -4 3 0 -2.60 6.00 4 3 0 2.90 6.40 4 3 0 4.10 4.40 -4 3 0 13.70 5.10 -4 3 0 1.40 8.90 -4 3 0 6.90 4.50 4 3 0 10.10 8.30 -4 3 0 5.60 6.70 -4 3 0 10.40 6.40 -4 3 0 13.90 11.40 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62.39 19.60 -9 3 0 77.49 12.80 9 3 0 63.79 15.40 -9 3 0 51.89 19.80 -9 3 0 87.79 17.80 9 3 0 67.79 25.50 -9 3 0 58.79 16.70 -9 3 0 60.19 22.10 -9 3 0 88.79 30.60 -9 3 0 77.19 20.40 9 3 0 117.69 26.90 -10 -3 0 283.97 38.50 -10 -3 0 293.97 50.59 -10 -3 0 327.97 24.20 -10 -3 0 225.08 46.20 -10 -3 0 336.57 46.90 10 -3 0 338.57 28.00 -10 3 0 318.37 49.10 10 3 0 323.57 49.10 -10 3 0 265.97 44.70 -10 3 0 269.57 23.40 -10 3 0 309.37 35.20 -10 3 0 309.37 43.90 10 3 0 293.87 32.30 -10 3 0 274.47 38.20 -10 3 0 373.86 66.19 11 -3 0 12.40 9.70 -11 -3 0 11.60 15.40 -11 -3 0 5.20 5.90 -11 -3 0 -2.50 10.40 -11 -3 0 -2.70 14.80 -11 3 0 -5.00 11.00 -11 3 0 12.50 15.00 -11 3 0 0.30 6.70 -11 3 0 2.20 9.80 -11 3 0 12.40 13.30 11 3 0 -8.70 9.00 -12 -3 0 245.18 40.60 -12 -3 0 310.77 51.79 -12 -3 0 241.18 53.09 -12 -3 0 312.07 23.30 12 -3 0 264.87 31.00 -12 3 0 248.88 41.00 -12 3 0 329.67 49.20 -12 3 0 271.67 23.60 -12 3 0 297.27 52.49 12 3 0 290.27 34.00 13 -3 0 111.09 21.40 -13 -3 0 155.88 16.90 -13 -3 0 136.39 31.70 -13 -3 0 96.39 36.20 -13 -3 0 132.39 35.10 13 3 0 173.98 26.80 -13 3 0 129.99 17.30 -13 3 0 113.59 30.60 -14 -3 0 138.89 44.00 -14 -3 0 124.69 34.50 14 3 0 91.09 21.20 -14 3 0 174.38 39.60 -14 3 0 137.29 42.70 0 -4 0 230.28 17.20 0 -4 0 237.18 15.80 0 -4 0 267.57 20.20 0 -4 0 235.08 14.60 0 -4 0 228.48 16.30 0 -4 0 260.87 15.50 0 -4 0 279.47 21.20 0 -4 0 280.37 19.00 0 -4 0 244.28 15.50 0 -4 0 231.68 16.50 0 4 0 213.78 18.80 0 4 0 274.97 19.40 0 4 0 229.38 15.20 0 4 0 256.37 15.20 0 4 0 251.77 16.60 0 4 0 248.08 17.20 0 4 0 255.97 20.70 0 4 0 239.68 17.70 0 4 0 274.17 20.20 0 4 0 259.97 15.30 0 4 0 252.77 16.10 -1 -4 0 41.60 7.90 -1 -4 0 30.20 8.70 1 -4 0 30.40 7.00 -1 -4 0 47.40 8.50 1 -4 0 19.10 7.80 -1 -4 0 32.40 6.30 -1 -4 0 46.70 10.30 1 -4 0 39.20 7.40 -1 -4 0 44.20 11.80 -1 -4 0 49.40 9.40 -1 -4 0 28.30 9.60 1 -4 0 33.40 10.50 1 -4 0 52.79 6.30 1 -4 0 35.40 7.70 1 -4 0 49.10 11.00 1 -4 0 30.30 6.30 -1 -4 0 37.60 8.50 1 -4 0 48.70 7.80 -1 -4 0 39.20 7.50 -1 4 0 40.20 5.60 1 4 0 56.59 9.40 1 4 0 42.20 8.00 1 4 0 43.70 9.60 -1 4 0 47.80 10.50 1 4 0 32.60 9.40 1 4 0 35.00 7.90 1 4 0 28.50 8.80 1 4 0 35.90 6.90 -1 4 0 40.60 7.10 1 4 0 37.70 12.20 -1 4 0 38.90 6.50 -1 4 0 32.10 7.40 -1 4 0 49.40 11.70 1 4 0 52.19 8.30 -1 4 0 43.30 8.10 -1 4 0 44.20 5.20 -2 -4 0 2902.01 135.39 2 -4 0 2959.00 127.99 2 -4 0 2848.81 123.09 -2 -4 0 2904.41 130.09 -2 -4 0 2984.50 132.29 2 -4 0 2978.90 127.49 2 -4 0 2906.91 133.09 2 -4 0 2959.30 137.09 2 -4 0 2868.71 126.49 -2 -4 0 3022.20 131.79 -2 -4 0 2873.51 127.69 -2 -4 0 3080.99 130.79 -2 -4 0 3039.60 131.69 -2 -4 0 2968.90 143.99 -2 -4 0 2872.31 132.19 -2 4 0 2940.51 128.09 2 4 0 2899.31 127.29 -2 4 0 2865.91 125.89 -2 4 0 2930.71 129.49 -2 4 0 2944.91 132.79 2 4 0 2988.00 145.49 2 4 0 2914.41 130.89 2 4 0 3015.30 132.59 -2 4 0 2975.70 136.99 2 4 0 2905.91 131.89 -2 4 0 3043.60 131.29 -2 4 0 2837.42 127.09 -2 4 0 2847.71 122.69 -2 4 0 2828.92 133.59 2 4 0 3030.60 131.69 2 4 0 2962.50 131.09 -3 -4 0 1429.96 86.59 3 -4 0 1393.26 65.49 3 -4 0 1341.77 64.69 -3 -4 0 1466.15 66.19 -3 -4 0 1458.65 71.39 -3 -4 0 1407.26 76.79 3 -4 0 1377.26 76.79 -3 -4 0 1383.66 72.99 3 -4 0 1495.05 72.59 3 -4 0 1368.86 68.39 3 -4 0 1364.36 61.99 -3 -4 0 1454.55 72.79 -3 -4 0 1369.36 72.39 -3 4 0 1361.26 67.69 3 4 0 1372.66 64.89 3 4 0 1368.26 70.59 -3 4 0 1395.16 65.79 -3 4 0 1426.46 69.89 3 4 0 1434.76 88.19 -3 4 0 1402.06 64.79 3 4 0 1347.57 71.69 -3 4 0 1499.15 62.19 -3 4 0 1396.26 73.79 -3 4 0 1463.05 77.19 3 4 0 1374.26 68.79 3 4 0 1346.67 71.99 -3 4 0 1415.86 67.99 -3 4 0 1364.76 71.19 -3 4 0 1377.86 62.59 -4 -4 0 174.58 24.30 -4 -4 0 226.78 37.70 4 -4 0 167.58 21.20 -4 -4 0 185.48 24.60 -4 -4 0 146.49 15.70 -4 -4 0 193.28 23.40 -4 -4 0 188.98 27.30 4 -4 0 187.38 14.90 4 -4 0 188.28 15.70 4 -4 0 173.28 26.20 4 -4 0 196.58 15.10 -4 4 0 164.28 13.20 -4 4 0 192.28 26.30 4 4 0 175.98 14.60 -4 4 0 177.68 15.40 -4 4 0 203.38 24.60 4 4 0 149.39 22.40 -4 4 0 191.38 27.90 4 4 0 208.18 23.10 4 4 0 234.68 26.70 -4 4 0 174.18 14.30 -4 4 0 190.98 16.80 -4 4 0 186.38 22.10 -4 4 0 190.08 14.70 4 4 0 211.38 21.20 -4 4 0 187.08 15.30 -5 -4 0 9.40 11.60 5 -4 0 33.20 11.20 -5 -4 0 27.20 7.60 5 -4 0 37.80 7.80 -5 -4 0 25.30 11.90 5 -4 0 32.60 8.60 -5 -4 0 51.69 24.80 -5 -4 0 20.70 11.20 -5 -4 0 28.60 14.80 5 -4 0 31.70 8.60 5 4 0 30.80 7.50 -5 4 0 15.40 7.50 -5 4 0 26.50 10.50 -5 4 0 10.50 9.50 -5 4 0 25.80 7.60 -5 4 0 10.50 13.00 5 4 0 41.50 12.10 -5 4 0 27.00 6.80 -5 4 0 36.80 8.90 5 4 0 24.30 10.40 -5 4 0 20.20 8.10 5 4 0 31.00 14.30 -5 4 0 28.10 7.40 5 4 0 30.80 13.00 -5 4 0 38.20 14.30 6 -4 0 583.94 46.60 -6 -4 0 588.34 50.09 -6 -4 0 581.74 63.99 -6 -4 0 677.93 37.30 -6 -4 0 638.84 45.20 6 -4 0 628.04 35.30 6 -4 0 689.63 37.80 -6 -4 0 668.23 49.60 -6 4 0 641.14 38.80 6 4 0 576.54 46.10 6 4 0 685.93 35.10 -6 4 0 615.94 52.59 6 4 0 638.84 44.20 6 4 0 629.44 50.39 -6 4 0 644.04 52.99 -6 4 0 704.63 41.90 -6 4 0 627.54 47.30 -6 4 0 601.24 36.40 -6 4 0 551.44 44.00 6 4 0 645.94 41.40 -6 4 0 621.34 36.30 7 -4 0 96.09 21.30 -7 -4 0 72.09 19.30 -7 -4 0 82.69 31.50 -7 -4 0 97.39 26.20 7 -4 0 76.39 11.30 -7 -4 0 63.89 12.10 7 -4 0 70.99 13.10 -7 -4 0 80.49 23.70 7 4 0 123.69 27.20 7 4 0 74.89 10.80 -7 4 0 93.29 20.10 7 4 0 95.59 21.00 -7 4 0 82.29 16.00 -7 4 0 83.19 12.70 -7 4 0 48.40 19.30 -7 4 0 53.29 12.10 7 4 0 95.69 19.60 7 4 0 47.60 12.70 -7 4 0 62.39 18.50 -7 4 0 83.89 15.60 -7 4 0 72.59 24.90 8 -4 0 945.91 49.80 -8 -4 0 808.92 61.59 -8 -4 0 942.91 94.49 8 -4 0 1015.50 70.89 -8 -4 0 954.20 74.89 -8 -4 0 1052.99 53.89 -8 -4 0 1085.69 81.49 8 -4 0 968.50 53.99 -8 -4 0 951.30 69.09 8 4 0 1003.60 73.19 -8 4 0 984.50 52.59 -8 4 0 937.31 73.09 -8 4 0 994.30 70.79 8 4 0 969.30 48.30 -8 4 0 986.00 55.99 -8 4 0 972.70 64.79 -8 4 0 1034.50 62.29 8 4 0 1071.89 69.79 -8 4 0 969.30 57.99 8 4 0 1044.30 59.39 8 4 0 922.01 62.99 -8 4 0 1016.80 79.49 -9 -4 0 25.50 8.80 9 -4 0 11.30 8.00 -9 -4 0 22.20 18.50 -9 -4 0 22.50 24.70 9 -4 0 11.80 5.20 -9 -4 0 12.00 11.90 -9 -4 0 25.70 17.70 -9 -4 0 25.00 15.70 9 -4 0 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45.80 -1 -5 0 730.33 37.20 1 -5 0 736.13 38.10 -1 -5 0 683.73 43.60 -1 5 0 730.63 40.10 -1 5 0 755.12 41.10 1 5 0 731.83 39.20 -1 5 0 718.73 43.50 1 5 0 738.53 43.90 1 5 0 797.72 42.90 1 5 0 704.93 40.30 1 5 0 789.92 40.90 -1 5 0 713.93 44.00 1 5 0 766.92 44.40 -1 5 0 761.22 35.80 1 5 0 742.33 40.10 1 5 0 805.72 49.30 -1 5 0 746.33 46.60 -1 5 0 770.82 38.60 1 5 0 756.92 38.40 -1 5 0 805.22 38.80 -1 5 0 746.53 36.30 2 -5 0 2103.09 107.69 -2 -5 0 2195.98 97.99 2 -5 0 2110.59 102.79 2 -5 0 2186.18 92.09 2 -5 0 2216.78 103.89 -2 -5 0 2176.28 112.69 -2 -5 0 2151.78 99.99 -2 -5 0 2236.88 100.39 -2 -5 0 2211.28 101.19 -2 -5 0 2051.29 97.89 2 -5 0 2190.38 98.79 2 -5 0 2166.38 98.09 -2 -5 0 2193.88 102.09 2 -5 0 2191.08 97.49 -2 -5 0 2202.58 102.29 2 -5 0 2121.79 94.49 -2 -5 0 2168.08 105.09 2 5 0 2134.59 100.99 2 5 0 2270.37 101.99 -2 5 0 2040.60 106.49 -2 5 0 2248.18 103.29 -2 5 0 2109.99 91.99 -2 5 0 2254.77 98.89 2 5 0 2088.79 99.19 2 5 0 2114.29 101.69 -2 5 0 2231.58 97.79 -2 5 0 2185.68 97.59 2 5 0 2043.80 96.89 2 5 0 2082.79 100.99 2 5 0 2167.18 114.29 -2 5 0 2033.40 100.99 -2 5 0 2148.58 98.29 -3 -5 0 140.89 22.60 -3 -5 0 184.98 16.80 -3 -5 0 259.47 25.90 3 -5 0 225.38 17.10 3 -5 0 219.08 25.80 -3 -5 0 250.67 26.70 -3 -5 0 243.98 26.30 3 -5 0 186.68 17.10 -3 -5 0 222.48 24.20 -3 -5 0 138.79 27.70 3 -5 0 206.08 17.50 3 -5 0 225.38 13.80 3 -5 0 236.28 29.40 -3 5 0 201.38 16.70 -3 5 0 214.88 21.70 3 5 0 188.88 22.60 -3 5 0 224.48 12.70 3 5 0 221.58 35.60 -3 5 0 189.18 17.00 -3 5 0 183.18 20.60 -3 5 0 183.38 16.00 -3 5 0 218.08 24.50 3 5 0 203.48 16.60 -3 5 0 208.38 12.40 -3 5 0 272.37 32.20 3 5 0 195.68 22.30 3 5 0 251.37 25.40 -3 5 0 229.48 22.80 3 5 0 250.27 26.50 -4 -5 0 53.29 12.70 -4 -5 0 42.20 14.10 4 -5 0 78.49 21.10 -4 -5 0 35.10 13.10 4 -5 0 56.29 10.30 -4 -5 0 54.99 10.70 4 -5 0 53.19 12.30 -4 -5 0 57.59 14.60 -4 -5 0 53.39 16.60 4 5 0 47.00 14.20 -4 5 0 57.49 8.60 4 5 0 48.80 12.80 -4 5 0 57.59 10.60 -4 5 0 44.70 10.80 -4 5 0 37.90 15.80 4 5 0 65.79 13.50 -4 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21 0 4.50 12.20 -7 21 0 -4.90 12.30 7 21 0 2.00 31.30 -8 -21 0 124.49 36.80 8 -21 0 134.79 48.90 -8 -21 0 56.69 24.30 8 -21 0 140.39 46.70 -8 -21 0 107.19 42.50 -8 -21 0 152.08 44.20 -8 -21 0 90.29 35.50 -8 21 0 98.59 29.20 -8 21 0 165.38 35.30 8 21 0 80.69 33.60 -8 21 0 92.39 33.80 -9 -21 0 36.20 26.30 -9 -21 0 71.39 28.10 -9 -21 0 40.10 29.40 9 -21 0 24.20 32.60 -9 -21 0 53.79 27.30 -9 -21 0 132.99 32.10 -9 21 0 -3.20 22.80 -9 21 0 36.60 19.10 9 21 0 80.09 35.90 -9 21 0 96.39 30.40 -10 -21 0 96.49 34.90 -10 -21 0 145.09 43.30 10 -21 0 90.79 46.70 -10 -21 0 99.69 43.20 -10 -21 0 73.79 23.90 -10 -21 0 89.29 33.00 -10 21 0 124.69 32.90 -10 21 0 150.78 36.50 10 21 0 141.69 40.90 0 -22 0 882.01 93.39 0 -22 0 868.01 68.79 0 -22 0 839.72 60.69 0 -22 0 829.92 58.99 0 -22 0 825.02 69.89 0 -22 0 856.41 69.39 0 -22 0 892.61 65.59 0 -22 0 899.91 57.99 0 -22 0 963.60 104.69 0 -22 0 735.33 102.99 0 -22 0 875.81 64.09 0 22 0 932.91 98.69 0 22 0 757.02 67.39 0 22 0 885.01 66.09 0 22 0 773.22 80.59 0 22 0 884.81 62.39 -1 -22 0 114.19 27.30 -1 -22 0 116.79 28.30 -1 -22 0 123.59 28.30 1 -22 0 104.29 36.20 -1 -22 0 91.89 19.70 1 -22 0 47.50 27.40 -1 -22 0 123.59 30.80 1 -22 0 151.18 25.10 -1 -22 0 99.89 24.70 1 -22 0 80.39 20.50 -1 -22 0 47.30 31.60 -1 -22 0 78.19 34.20 1 -22 0 138.99 24.50 -1 -22 0 65.79 18.20 -1 -22 0 64.79 37.70 1 -22 0 70.79 23.50 1 -22 0 65.69 50.69 1 -22 0 125.49 25.10 1 -22 0 138.89 27.80 1 -22 0 171.68 34.10 -1 22 0 111.89 24.70 -1 22 0 84.89 21.80 1 22 0 65.39 23.00 -1 22 0 70.39 22.40 1 22 0 99.09 24.90 1 22 0 97.39 43.90 -1 22 0 84.29 27.30 -1 22 0 103.19 33.90 1 22 0 80.19 34.40 1 22 0 97.29 34.50 1 22 0 104.29 25.30 -1 22 0 187.88 45.40 1 22 0 78.79 35.30 2 -22 0 3.00 9.00 2 -22 0 0.00 11.80 2 -22 0 11.40 18.00 -2 -22 0 37.80 18.90 -2 -22 0 19.90 11.40 2 -22 0 -0.50 10.10 2 -22 0 9.30 14.30 -2 -22 0 10.10 12.70 2 -22 0 7.50 12.30 -2 -22 0 -22.90 15.60 -2 -22 0 -4.80 12.20 -2 -22 0 -8.70 14.40 -2 -22 0 57.39 22.70 -2 -22 0 11.80 10.90 2 -22 0 3.90 18.10 -2 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29.30 4 -22 0 86.99 35.50 -4 22 0 41.10 18.80 4 22 0 48.50 28.50 4 22 0 64.49 22.40 4 22 0 87.99 41.80 4 22 0 34.40 21.10 -4 22 0 63.09 22.80 -4 22 0 27.60 20.90 -5 -22 0 8.90 15.20 -5 -22 0 28.40 23.70 -5 -22 0 58.29 29.90 -5 -22 0 14.80 19.40 5 -22 0 33.60 29.60 -5 -22 0 9.10 17.40 5 -22 0 23.70 25.50 -5 -22 0 17.70 29.70 5 22 0 51.59 22.60 -5 22 0 38.10 20.10 -5 22 0 -1.30 12.90 -5 22 0 29.70 21.60 5 22 0 10.60 31.20 5 22 0 34.80 23.80 5 22 0 28.10 24.60 -6 -22 0 151.38 37.60 -6 -22 0 247.38 73.79 -6 -22 0 154.98 42.20 -6 -22 0 243.28 45.70 6 -22 0 177.48 54.49 6 -22 0 224.18 51.79 -6 -22 0 143.39 39.20 -6 -22 0 162.88 42.30 -6 22 0 194.78 36.50 6 22 0 285.27 53.59 -6 22 0 118.29 29.20 6 22 0 183.88 56.49 6 22 0 273.97 49.90 -6 22 0 193.48 43.50 -7 -22 0 20.80 21.30 -7 -22 0 -16.40 12.00 -7 -22 0 1.30 18.70 -7 -22 0 -8.00 15.80 7 -22 0 19.10 30.10 -7 -22 0 -26.70 14.70 -7 22 0 -7.00 12.40 7 22 0 -4.70 29.20 -7 22 0 33.70 18.30 -7 22 0 8.30 13.90 7 22 0 -3.40 21.80 -8 -22 0 213.38 46.50 -8 -22 0 214.68 40.60 -8 -22 0 230.28 54.79 8 -22 0 250.97 63.59 8 -22 0 213.28 52.09 -8 -22 0 175.98 43.50 -8 -22 0 215.68 49.00 8 22 0 187.58 47.30 -8 22 0 199.48 40.30 -8 22 0 246.28 49.40 -8 22 0 201.18 37.00 9 -22 0 156.28 54.19 -9 -22 0 115.59 31.80 -9 -22 0 99.99 32.30 -9 -22 0 144.39 47.20 -9 -22 0 212.38 49.30 -9 -22 0 142.19 40.70 -9 22 0 105.29 29.50 -9 22 0 150.98 38.00 9 22 0 216.98 51.89 -9 22 0 156.78 43.70 0 -23 0 -5.00 10.90 0 -23 0 15.90 15.10 0 -23 0 -8.80 17.60 0 -23 0 9.10 11.90 0 -23 0 0.60 19.20 0 -23 0 -59.59 27.60 0 -23 0 3.70 10.90 0 -23 0 -12.20 7.70 0 -23 0 12.50 17.60 0 23 0 21.50 14.80 0 23 0 6.90 16.90 0 23 0 -13.60 17.40 0 23 0 23.90 16.40 0 23 0 11.00 14.00 0 23 0 24.30 22.00 -1 -23 0 8.50 10.70 1 -23 0 18.00 18.50 1 -23 0 43.80 16.70 -1 -23 0 22.30 17.10 -1 -23 0 19.40 16.00 -1 -23 0 36.50 21.70 1 -23 0 110.59 37.90 -1 -23 0 28.50 18.00 1 -23 0 27.90 16.30 1 -23 0 24.90 24.30 1 -23 0 42.80 15.30 1 -23 0 42.90 30.90 -1 -23 0 70.39 32.20 -1 -23 0 39.00 28.90 1 -23 0 37.40 18.10 -1 -23 0 48.60 26.60 1 -23 0 -1.80 21.20 -1 23 0 41.50 25.40 1 23 0 36.30 17.40 -1 23 0 50.49 19.20 -1 23 0 1.70 23.00 -1 23 0 63.69 23.70 1 23 0 15.30 22.00 -1 23 0 20.40 18.50 1 23 0 70.69 25.50 -1 23 0 36.80 17.70 1 23 0 -22.20 17.60 1 23 0 25.80 17.50 2 -23 0 9.50 14.90 -2 -23 0 13.20 12.00 -2 -23 0 19.10 15.60 2 -23 0 -0.70 20.50 -2 -23 0 11.00 19.90 2 -23 0 25.90 28.30 -2 -23 0 17.10 24.20 -2 -23 0 0.80 14.70 2 -23 0 -1.40 10.20 -2 -23 0 17.60 16.30 2 -23 0 16.80 13.00 2 -23 0 -22.10 20.30 -2 -23 0 18.50 15.70 -2 -23 0 11.40 16.50 -2 23 0 36.50 21.20 -2 23 0 6.20 17.30 2 23 0 23.20 25.40 2 23 0 12.60 22.70 2 23 0 22.30 16.40 -2 23 0 -6.70 11.30 -2 23 0 21.40 17.40 2 23 0 -11.70 14.10 -3 -23 0 -1.00 17.10 -3 -23 0 19.60 19.10 -3 -23 0 31.40 19.00 3 -23 0 106.19 58.39 -3 -23 0 1.40 15.40 3 -23 0 0.50 12.70 3 -23 0 -9.70 20.90 3 -23 0 17.50 27.80 3 -23 0 21.70 12.60 3 -23 0 25.50 13.90 -3 -23 0 37.80 17.30 -3 -23 0 12.00 15.70 -3 -23 0 -5.30 11.90 -3 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51.69 4 7 -2 770.22 47.90 4 7 -2 812.52 55.19 -4 7 2 795.52 40.30 -4 7 2 809.22 48.40 -4 7 2 837.62 55.49 4 7 -2 796.42 55.99 4 7 -2 756.92 52.89 -4 7 2 763.82 56.29 -4 7 2 818.12 48.30 4 7 -2 854.91 52.49 -4 7 2 709.83 60.39 4 7 -2 807.32 49.00 4 7 -2 768.72 56.49 4 7 -2 768.12 55.39 -4 7 2 750.92 48.30 3 -7 -2 759.32 47.40 -3 -7 2 749.62 49.70 3 -7 -2 698.43 44.70 -3 -7 2 752.92 52.49 3 -7 -2 797.12 49.50 3 -7 -2 764.22 39.30 3 -7 -2 667.03 52.59 -3 -7 2 698.43 43.30 -3 -7 2 835.92 49.80 3 -7 -2 780.02 35.40 3 -7 -2 798.32 35.90 -3 -7 2 841.62 53.09 3 -7 -2 700.73 46.00 -3 -7 2 813.62 49.90 -3 -7 2 833.42 48.40 -3 -7 2 772.72 48.00 3 -7 -2 768.82 55.49 -3 -7 2 823.22 61.49 -3 -7 2 759.42 48.50 3 7 -2 748.93 46.40 3 7 -2 799.82 53.49 3 7 -2 800.72 52.29 -3 7 2 775.42 48.40 3 7 -2 822.02 53.49 3 7 -2 804.42 43.60 -3 7 2 805.72 40.00 3 7 -2 706.13 50.39 -3 7 2 695.23 49.00 -3 7 2 847.22 47.50 -3 7 2 751.32 46.30 3 7 -2 729.43 47.60 3 7 -2 839.72 50.99 -3 7 2 707.53 52.59 3 7 -2 783.52 52.79 -2 -7 2 125.39 18.70 2 -7 -2 127.49 14.00 2 -7 -2 109.59 11.50 -2 -7 2 127.49 18.40 -2 -7 2 105.39 18.40 -2 -7 2 84.29 16.30 -2 -7 2 92.89 20.30 -2 -7 2 106.99 16.70 2 -7 -2 52.99 18.60 -2 -7 2 93.69 15.90 -2 -7 2 86.59 20.80 -2 -7 2 113.49 18.60 2 -7 -2 66.29 16.80 -2 -7 2 130.29 19.00 2 -7 -2 127.99 23.20 2 -7 -2 90.29 15.10 2 -7 -2 110.49 13.30 2 -7 -2 133.79 18.80 2 -7 -2 121.09 19.30 2 7 -2 139.69 20.70 2 7 -2 107.79 17.60 2 7 -2 143.59 21.30 -2 7 2 116.69 20.80 -2 7 2 132.59 17.10 2 7 -2 117.89 19.60 -2 7 2 121.79 14.30 2 7 -2 90.89 22.10 2 7 -2 125.59 18.30 -2 7 2 142.79 18.60 -2 7 2 104.39 13.20 -2 7 2 125.69 19.10 2 7 -2 81.59 15.50 2 7 -2 133.69 19.70 -2 7 2 91.79 14.80 2 7 -2 97.59 20.40 2 7 -2 96.39 18.20 -2 7 2 118.79 17.60 1 -7 -2 1892.71 103.89 -1 -7 2 2029.40 96.99 1 -7 -2 1928.41 97.19 -1 -7 2 1913.71 96.49 -1 -7 2 1951.40 101.89 -1 -7 2 2188.48 105.19 1 -7 -2 1993.30 92.89 -1 -7 2 2122.39 100.79 -1 -7 2 1977.10 95.49 1 -7 -2 1991.60 96.49 -1 -7 2 2119.49 96.49 1 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14 4.20 22.90 -3 7 14 -1.70 22.90 3 7 -14 -6.70 24.40 -3 7 14 71.59 31.60 -2 -7 14 32.50 25.10 -2 -7 14 32.30 23.50 -2 -7 14 32.60 25.00 2 7 -14 42.50 33.10 -2 7 14 -2.70 19.50 -2 7 14 58.39 31.40 -2 7 14 -20.00 19.40 -2 7 14 24.20 25.60 -1 -7 14 58.49 36.60 -1 -7 14 49.60 27.70 -1 -7 14 7.70 18.60 -1 7 14 6.50 21.40 -1 7 14 84.89 36.50 -1 7 14 63.19 49.40 1 7 -14 82.39 36.10 -1 7 14 54.89 32.20 0 -7 14 23.00 26.10 0 -7 14 30.30 26.00 0 7 -14 -12.90 21.30 0 7 14 20.00 29.60 0 7 14 -5.40 18.40 0 7 14 23.90 23.80 1 -7 14 -17.00 18.20 1 -7 14 -18.30 19.00 -1 7 -14 12.90 24.80 1 7 14 0.80 19.00 1 7 14 3.60 26.10 -7 -8 14 -12.50 18.80 -7 -8 14 16.30 21.90 -7 -8 14 -11.20 34.90 7 -8 -14 -12.30 24.60 -7 8 14 8.80 16.80 7 8 -14 -52.29 18.00 -7 8 14 -26.90 18.60 -7 8 14 -27.60 22.80 6 -8 -14 61.79 35.30 -6 -8 14 85.59 32.80 -6 -8 14 50.49 28.90 -6 -8 14 82.99 45.90 -6 8 14 89.19 35.00 -6 8 14 86.69 37.30 6 8 -14 77.99 41.10 -6 8 14 76.99 34.60 -6 8 14 135.09 37.30 -5 -8 14 105.29 34.80 -5 -8 14 80.69 32.00 -5 -8 14 160.78 48.60 -5 8 14 104.09 35.70 -5 8 14 155.08 42.70 5 8 -14 230.38 58.59 -5 8 14 128.49 40.20 -5 8 14 185.98 46.30 -4 -8 14 200.08 50.39 -4 -8 14 158.68 42.30 -4 -8 14 120.09 37.50 -4 8 14 172.28 44.70 -4 8 14 151.48 45.20 -4 8 14 122.99 38.20 -4 8 14 201.88 50.09 4 8 -14 99.99 35.40 4 8 -14 99.19 42.40 -3 -8 14 92.49 36.20 -3 -8 14 46.10 29.00 -3 -8 14 53.39 28.00 -3 8 14 129.69 41.90 -3 8 14 69.19 32.40 3 8 -14 84.29 39.00 -3 8 14 33.80 25.40 -3 8 14 81.89 36.40 3 8 -14 59.09 34.40 -2 -8 14 34.70 29.70 -2 -8 14 35.30 25.20 -2 -8 14 33.70 23.50 2 8 -14 20.70 27.40 -2 8 14 38.30 27.80 -2 8 14 22.50 23.60 -2 8 14 45.70 32.10 -2 8 14 53.69 28.80 -1 -8 14 29.60 24.50 -1 -8 14 30.20 28.10 -1 8 14 -3.70 19.30 -1 8 14 -14.10 22.00 -1 8 14 25.90 22.10 1 8 -14 -23.80 19.90 0 -8 14 6.70 22.90 0 -8 14 76.59 34.00 0 8 14 59.69 33.60 0 8 14 22.60 25.40 0 8 -14 22.20 26.20 0 8 14 38.60 31.10 1 -8 14 32.40 27.00 1 -8 14 63.29 30.60 1 8 14 43.40 33.00 1 8 14 68.69 36.10 -1 8 -14 73.39 34.70 -7 -9 14 71.39 57.09 -7 -9 14 88.19 35.10 7 -9 -14 121.89 42.80 -7 -9 14 170.98 41.80 7 9 -14 133.79 48.00 -7 9 14 100.69 36.50 -7 9 14 131.29 49.70 -7 9 14 154.28 39.40 -6 -9 14 2.30 37.50 -6 -9 14 56.89 28.70 -6 -9 14 63.19 30.60 6 -9 -14 -21.30 21.40 -6 9 14 66.29 29.70 -6 9 14 38.50 27.50 -6 9 14 57.19 25.80 6 9 -14 18.30 31.80 -6 9 14 11.90 23.10 -5 -9 14 6.20 24.00 -5 -9 14 -16.30 23.70 -5 -9 14 -7.30 18.70 -5 9 14 28.70 18.50 -5 9 14 42.10 29.50 5 9 -14 -18.30 26.30 -5 9 14 40.40 20.80 -5 9 14 23.40 24.60 5 9 -14 8.10 24.90 -4 -9 14 14.40 22.80 -4 -9 14 -12.30 23.00 -4 -9 14 0.90 21.20 -4 9 14 31.10 22.40 -4 9 14 9.50 20.20 4 9 -14 9.10 27.10 4 9 -14 46.50 37.50 -4 9 14 33.60 22.40 -4 9 14 8.10 20.50 -3 -9 14 41.70 29.50 -3 -9 14 -28.30 13.00 -3 -9 14 14.40 19.70 -3 9 14 29.20 27.60 -3 9 14 2.30 15.70 3 9 -14 42.40 33.80 3 9 -14 -13.60 19.10 -3 9 14 18.60 18.60 -3 9 14 24.60 23.50 -2 -9 14 39.70 25.80 -2 -9 14 22.80 24.20 -2 -9 14 5.50 19.20 -2 9 14 -28.80 16.20 -2 9 14 19.60 23.50 -2 9 14 36.70 27.40 -2 9 14 13.50 23.00 2 9 -14 10.60 29.50 -1 -9 14 -6.80 16.40 -1 -9 14 2.30 18.40 1 9 -14 -8.50 22.80 -1 9 14 8.70 23.80 -1 9 14 0.10 20.10 -1 9 14 -14.40 18.80 -1 9 14 17.50 21.30 0 -9 14 5.00 20.30 0 -9 14 -18.10 17.00 0 9 14 -7.00 20.60 0 9 14 3.10 23.60 0 9 14 28.00 42.70 0 9 -14 23.10 27.80 1 -9 14 56.39 29.20 1 -9 14 13.20 23.70 1 9 14 12.60 24.70 -1 9 -14 40.90 31.00 -6 -10 14 6.70 21.00 -6 -10 14 -4.10 17.30 6 -10 -14 -1.50 25.30 -6 -10 14 -47.50 33.90 -6 10 14 23.20 24.30 -6 10 14 29.90 23.00 -6 10 14 -30.40 15.60 6 10 -14 22.00 31.20 -6 10 14 39.20 23.00 -5 -10 14 -0.90 17.30 -5 -10 14 -13.70 17.00 -5 10 14 22.10 19.90 -5 10 14 22.10 24.60 5 10 -14 11.60 26.70 5 10 -14 2.10 28.10 -5 10 14 45.10 23.20 -5 10 14 29.80 26.80 -4 -10 14 47.30 25.00 -4 -10 14 41.80 28.20 -4 -10 14 38.60 28.10 -4 10 14 5.30 23.70 -4 10 14 51.79 26.10 -4 10 14 36.40 27.70 4 10 -14 55.19 30.70 -4 10 14 68.09 29.80 4 10 -14 41.20 34.30 -3 -10 14 -18.90 13.60 -3 -10 14 30.20 20.40 -3 -10 14 9.30 22.40 -3 10 14 20.40 26.00 -3 10 14 25.00 25.20 3 10 -14 -21.00 20.00 3 10 -14 11.50 27.40 -3 10 14 32.50 27.00 -3 10 14 17.30 21.80 -2 -10 14 -5.20 16.80 -2 -10 14 4.70 18.30 -2 10 14 23.00 29.90 -2 10 14 14.70 20.10 -2 10 14 6.10 25.30 -2 10 14 34.80 23.40 2 10 -14 10.20 26.50 -1 -10 14 97.99 36.00 -1 -10 14 72.09 33.00 -1 10 14 109.09 40.70 -1 10 14 118.39 41.90 1 10 -14 15.50 27.20 -1 10 14 83.99 37.70 0 -10 14 4.90 19.00 0 -10 14 16.20 24.60 0 10 14 7.90 22.30 0 10 14 15.30 28.00 0 10 -14 -20.90 20.40 0 10 14 59.09 33.90 6 -11 -14 94.69 42.30 -6 -11 14 145.89 40.90 6 11 -14 327.27 68.09 -6 11 14 242.68 57.19 5 -11 -14 -28.10 24.30 -5 -11 14 11.50 34.30 -5 -11 14 36.40 24.70 -5 -11 14 14.20 23.40 5 11 -14 37.30 29.70 -5 11 14 29.40 22.90 -5 11 14 58.89 29.00 5 11 -14 32.70 35.60 -5 11 14 68.29 28.00 -5 11 14 20.60 29.60 -4 -11 14 4.00 21.50 -4 -11 14 3.60 22.90 -4 -11 14 -15.80 15.70 4 11 -14 -2.80 22.00 -4 11 14 -9.70 20.50 -4 11 14 48.90 24.80 -4 11 14 6.50 17.50 -4 11 14 -4.80 21.50 4 11 -14 18.90 31.90 -3 -11 14 -3.70 17.50 -3 -11 14 21.50 22.70 -3 11 14 16.00 23.00 -3 11 14 18.70 23.80 3 11 -14 -6.60 24.80 3 11 -14 -16.00 24.00 -3 11 14 15.10 24.70 -2 -11 14 -24.60 15.50 -2 -11 14 12.10 24.90 2 11 -14 -18.00 18.10 -2 11 14 -26.80 17.10 -2 11 14 52.69 29.20 -2 11 14 14.70 22.50 2 11 -14 37.30 29.80 -1 -11 14 113.09 37.70 -1 -11 14 53.99 30.70 -1 11 14 53.09 31.30 -1 11 14 77.59 32.50 -1 11 14 119.29 42.30 1 11 -14 32.00 32.20 -5 -12 14 49.40 30.00 5 -12 -14 18.30 29.80 -5 12 14 -0.50 23.40 5 12 -14 24.90 26.80 5 12 -14 127.59 49.60 -4 -12 14 119.49 40.10 -4 -12 14 182.78 44.30 -4 12 14 201.68 51.69 4 12 -14 137.09 49.40 -4 12 14 176.88 44.50 -4 12 14 124.19 45.30 4 12 -14 161.68 45.30 -3 -12 14 102.99 34.90 -3 -12 14 107.19 36.20 -3 12 14 111.29 40.70 3 12 -14 88.09 35.50 3 12 -14 124.69 43.90 -3 12 14 91.79 36.00 -3 12 14 99.59 40.60 -2 -12 14 148.99 41.70 -2 -12 14 165.48 44.80 -2 12 14 260.37 56.39 -2 12 14 124.79 43.10 2 12 -14 251.67 59.49 -2 12 14 140.69 45.00 2 12 -14 145.99 41.50 6 0 -15 -21.60 23.40 -6 0 15 19.70 18.60 -6 0 15 -3.10 21.60 -6 0 15 -22.30 15.80 -5 0 15 -2.10 17.80 -5 0 15 0.40 19.50 5 0 -15 1.90 28.50 -5 0 15 30.40 20.40 4 0 -15 5.30 26.10 -4 0 15 8.80 17.40 -4 0 15 -6.10 16.60 -4 0 15 -18.80 16.70 -3 0 15 0.00 20.40 -3 0 15 21.00 19.80 -3 0 15 17.80 25.00 3 0 -15 -2.80 23.70 -2 0 15 8.80 20.20 -2 0 15 19.50 25.00 -2 0 15 18.00 26.00 -1 0 15 64.69 30.70 -1 0 15 22.60 26.30 -1 0 15 -24.60 16.90 -6 -1 15 -5.10 16.60 -6 -1 15 15.40 24.20 6 -1 -15 35.70 32.60 -6 -1 15 1.80 16.40 -6 1 15 89.19 30.90 6 1 -15 -9.30 21.70 -6 1 15 23.60 25.00 -6 1 15 13.30 19.60 -5 -1 15 54.49 22.60 -5 -1 15 36.10 27.20 5 -1 -15 17.00 28.50 -5 1 15 33.50 20.50 -5 1 15 -5.60 17.30 5 1 -15 40.50 34.00 -5 1 15 0.70 23.50 4 -1 -15 -21.30 22.90 -4 -1 15 10.90 22.00 -4 -1 15 44.80 23.50 -4 -1 15 -11.90 16.00 -4 1 15 -4.50 20.00 -4 1 15 29.80 20.10 -4 1 15 -10.60 18.80 4 1 -15 -12.80 24.70 3 -1 -15 -9.70 33.20 -3 -1 15 2.80 24.60 -3 -1 15 34.50 23.20 -3 -1 15 -12.80 16.20 3 1 -15 -24.20 23.30 -3 1 15 4.10 20.60 -3 1 15 20.30 19.70 -3 1 15 -7.70 18.60 -2 -1 15 6.90 20.90 -2 -1 15 11.00 25.00 -2 -1 15 40.30 25.80 -2 1 15 16.10 21.00 -2 1 15 29.40 30.40 -2 1 15 45.60 26.80 2 1 -15 16.30 27.80 -1 -1 15 170.38 47.60 -1 -1 15 201.58 50.99 -1 -1 15 184.38 46.10 -1 1 15 223.48 53.89 -1 1 15 207.48 51.19 -1 1 15 184.38 49.50 -6 -2 15 3.40 22.10 -6 -2 15 -3.00 20.40 -6 -2 15 -29.90 12.90 6 -2 -15 76.99 38.60 -6 2 15 59.59 25.90 -6 2 15 13.30 26.40 6 2 -15 33.60 34.90 -6 2 15 -11.80 21.60 -5 -2 15 47.10 28.90 5 -2 -15 107.99 42.60 -5 -2 15 102.59 37.40 -5 -2 15 200.98 45.40 5 2 -15 86.89 41.90 -5 2 15 70.49 33.20 -5 2 15 135.59 40.10 -5 2 15 40.00 28.90 -4 -2 15 111.79 39.60 -4 -2 15 126.39 36.30 -4 -2 15 20.10 25.30 4 -2 -15 80.19 47.80 4 2 -15 34.10 30.00 -4 2 15 99.29 35.30 -4 2 15 86.79 34.30 -4 2 15 130.69 39.70 -3 -2 15 11.10 25.50 -3 -2 15 13.80 21.20 -3 -2 15 66.89 31.40 -3 2 15 45.70 26.70 3 2 -15 91.69 39.40 -3 2 15 53.59 30.90 -3 2 15 26.30 25.30 -2 -2 15 -8.10 16.50 -2 -2 15 38.00 24.10 -2 -2 15 51.39 28.60 2 2 -15 17.90 28.90 -2 2 15 51.99 29.00 -2 2 15 18.50 22.50 -2 2 15 26.30 27.60 -1 -2 15 18.90 26.70 -1 -2 15 -4.50 19.90 -1 -2 15 51.29 28.10 -1 2 15 18.60 26.60 -1 2 15 -0.80 20.50 1 2 -15 12.00 24.70 -1 2 15 29.50 25.00 -6 -3 15 101.79 37.30 -6 -3 15 162.98 43.10 6 -3 -15 59.49 34.40 -6 3 15 150.68 42.50 6 3 -15 127.99 46.70 -6 3 15 170.88 44.80 -5 -3 15 109.79 35.00 5 -3 -15 351.36 77.99 -5 -3 15 203.78 46.20 -5 -3 15 156.88 41.30 -5 3 15 192.28 50.99 -5 3 15 169.58 45.90 5 3 -15 241.68 56.89 -5 3 15 218.08 51.19 -4 -3 15 20.80 22.50 -4 -3 15 27.80 22.20 -4 -3 15 10.00 22.00 -4 3 15 5.90 21.10 4 3 -15 44.70 32.60 -4 3 15 50.39 24.80 -4 3 15 6.60 20.30 -3 -3 15 29.60 24.60 -3 -3 15 28.90 26.50 -3 -3 15 24.60 20.60 -3 3 15 59.99 28.50 3 3 -15 25.10 29.60 -3 3 15 -19.60 18.70 -3 3 15 -13.60 17.20 -2 -3 15 129.69 40.60 -2 -3 15 122.19 40.20 -2 -3 15 110.09 41.40 -2 3 15 68.39 33.70 -2 3 15 78.29 34.80 2 3 -15 67.89 34.80 -2 3 15 8.40 25.00 -1 -3 15 51.29 30.40 -1 -3 15 15.00 23.80 -1 -3 15 4.60 22.40 1 3 -15 18.00 28.00 -1 3 15 43.80 28.60 -1 3 15 -0.70 21.60 -1 3 15 7.30 28.30 -5 -4 15 13.90 23.30 -5 -4 15 -9.80 17.10 -5 -4 15 64.89 28.70 -5 4 15 19.10 20.30 5 4 -15 31.30 32.20 -5 4 15 -23.40 16.40 -5 4 15 5.30 23.10 -4 -4 15 2.50 19.20 -4 -4 15 15.60 24.30 -4 -4 15 43.60 23.70 -4 4 15 -10.40 20.00 4 4 -15 -14.00 25.80 -4 4 15 9.10 24.00 -4 4 15 51.19 27.00 -3 -4 15 63.59 31.70 -3 -4 15 111.59 34.80 -3 -4 15 68.79 35.60 3 4 -15 104.59 39.40 -3 4 15 23.80 25.40 -3 4 15 101.99 37.40 -3 4 15 70.09 31.40 -2 -4 15 18.30 21.90 -2 -4 15 26.40 21.70 -2 -4 15 35.80 30.00 -2 4 15 25.30 24.60 -2 4 15 -18.70 16.90 2 4 -15 4.70 27.00 -2 4 15 7.20 26.20 -1 -4 15 23.20 24.70 -1 -4 15 25.50 24.10 -1 -4 15 60.29 32.70 -1 4 15 7.40 21.40 1 4 -15 45.60 34.10 -1 4 15 57.99 32.20 -1 4 15 26.90 29.90 -5 -5 15 31.90 22.90 -5 -5 15 31.50 25.40 -5 -5 15 1.90 21.00 5 5 -15 -3.20 25.20 -5 5 15 53.99 30.30 -5 5 15 18.20 27.10 -5 5 15 34.60 22.10 -4 -5 15 35.50 21.00 -4 -5 15 12.90 24.40 -4 -5 15 21.80 23.70 -4 5 15 -3.20 21.70 -4 5 15 38.60 26.70 4 5 -15 47.50 34.70 -4 5 15 -23.90 18.40 -3 -5 15 8.70 20.40 -3 -5 15 -3.00 18.70 -3 -5 15 45.00 26.90 3 5 -15 28.90 31.60 -3 5 15 62.09 32.50 -3 5 15 8.40 24.00 -3 5 15 41.30 25.10 -2 -5 15 159.88 45.40 -2 -5 15 176.48 45.80 -2 -5 15 166.78 46.30 2 5 -15 104.39 41.10 -2 5 15 133.29 41.00 -2 5 15 155.38 48.00 -2 5 15 115.79 40.50 -4 -6 15 38.20 21.90 -4 -6 15 -25.90 15.30 -4 -6 15 30.60 25.40 -4 6 15 24.70 23.20 -4 6 15 30.70 29.30 -4 6 15 7.30 24.00 4 6 -15 68.09 40.50 -3 -6 15 -27.70 11.60 -3 -6 15 20.10 25.90 -3 -6 15 -15.40 11.30 3 6 -15 -16.00 21.80 -3 6 15 -9.90 16.20 -3 6 15 -0.80 15.10 -3 6 15 10.00 25.20 -2 -6 15 1.10 19.30 -2 -6 15 8.20 21.50 -2 6 15 8.00 24.20 2 6 -15 10.10 27.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 8298 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.48520(4) 0.63115(2) 0.46653(4) 0.01848(15) Uani 1 1 d . . . . . Cl2 Cl -0.15858(9) 0.49948(4) -0.03815(9) 0.0383(3) Uani 1 1 d . . . . . Cl1 Cl -0.31988(9) 0.48412(5) 0.09200(10) 0.0462(3) Uani 1 1 d . . . . . Cl3 Cl -0.14077(11) 0.41046(5) 0.10347(10) 0.0523(3) Uani 1 1 d . . . . . F6 F 0.6848(2) 0.79293(9) 0.8420(2) 0.0398(6) Uani 1 1 d . . . . . F5 F 0.51393(18) 0.76601(10) 0.80926(18) 0.0367(6) Uani 1 1 d . . . . . F4 F 0.6443(2) 0.72143(9) 0.90665(18) 0.0385(6) Uani 1 1 d . . . . . N3 N 0.5874(2) 0.67596(11) 0.5658(2) 0.0187(7) Uani 1 1 d . . . . . N4 N 0.3653(2) 0.68170(12) 0.4568(2) 0.0196(7) Uani 1 1 d . . . . . O2 O 0.0643(2) 0.48643(12) 0.2502(3) 0.0389(7) Uani 1 1 d . . . . . N2 N 0.6097(2) 0.58607(12) 0.4573(2) 0.0199(7) Uani 1 1 d . . . . . O1 O 0.0418(2) 0.54088(12) 0.3730(3) 0.0427(8) Uani 1 1 d . . . . . N1 N 0.3797(2) 0.58152(12) 0.3872(2) 0.0209(7) Uani 1 1 d . . . . . N00E N 0.0986(3) 0.52045(14) 0.3171(3) 0.0306(8) Uani 1 1 d . . . . . C14 C 0.5539(3) 0.71554(14) 0.6237(3) 0.0186(8) Uani 1 1 d . . . . . C16 C 0.3801(3) 0.73303(14) 0.4910(3) 0.0188(8) Uani 1 1 d . . . . . C11 C 0.6979(3) 0.66477(14) 0.6144(3) 0.0205(8) Uani 1 1 d . . . . . C9 C 0.7222(3) 0.60145(14) 0.4813(3) 0.0204(8) Uani 1 1 d . . . . . C3 C 0.2993(3) 0.50127(15) 0.3359(3) 0.0225(8) Uani 1 1 d . . . . . H3 H 0.291532 0.465113 0.320633 0.027 Uiso 1 1 calc R U . . . C8 C 0.7852(3) 0.56903(15) 0.4243(3) 0.0232(8) Uani 1 1 d . . . . . H8 H 0.862079 0.573202 0.421944 0.028 Uiso 1 1 calc R U . . . C13 C 0.6373(3) 0.72218(14) 0.7221(3) 0.0211(8) Uani 1 1 d . . . . . C46 C 0.6200(3) 0.75060(15) 0.8189(3) 0.0229(8) Uani 1 1 d . . . . . C4 C 0.4024(3) 0.53017(14) 0.3665(3) 0.0194(8) Uani 1 1 d . . . . . C6 C 0.6053(3) 0.54182(14) 0.3964(3) 0.0208(8) Uani 1 1 d . . . . . C25 C -0.0289(3) 0.62177(15) 0.0975(3) 0.0284(9) Uani 1 1 d . . . . . H25 H -0.039102 0.609129 0.026474 0.034 Uiso 1 1 calc R U . . . C15 C 0.4643(3) 0.74908(14) 0.5765(3) 0.0200(8) Uani 1 1 d . . . . . C12 C 0.7275(3) 0.69121(15) 0.7152(3) 0.0227(8) Uani 1 1 d . . . . . C21 C 0.0929(3) 0.63758(14) 0.2713(3) 0.0233(8) Uani 1 1 d . . . . . C26 C 0.0760(3) 0.61876(15) 0.1676(3) 0.0256(9) Uani 1 1 d . . . . . H26 H 0.137272 0.603586 0.144438 0.031 Uiso 1 1 calc R U . . . C7 C 0.7142(3) 0.53172(15) 0.3751(3) 0.0224(8) Uani 1 1 d . . . . . H7 H 0.732668 0.503798 0.333838 0.027 Uiso 1 1 calc R U . . . C2 C 0.2161(3) 0.53575(15) 0.3332(3) 0.0245(9) Uani 1 1 d . . . . . C28 C 0.4458(3) 0.45162(15) 0.2058(3) 0.0260(9) Uani 1 1 d . . . . . H28 H 0.389633 0.476401 0.175335 0.031 Uiso 1 1 calc R U . . . C10 C 0.7677(3) 0.63759(14) 0.5595(3) 0.0217(8) Uani 1 1 d . . . . . C39 C 0.4729(3) 0.80505(14) 0.6069(3) 0.0219(8) Uani 1 1 d . . . . . C1 C 0.2634(3) 0.58681(15) 0.3594(3) 0.0221(8) Uani 1 1 d . . . . . C27 C 0.5169(3) 0.46159(14) 0.3056(3) 0.0217(8) Uani 1 1 d . . . . . C23 C -0.1035(3) 0.66159(16) 0.2342(3) 0.0306(10) Uani 1 1 d . . . . . H23 H -0.165631 0.676045 0.257210 0.037 Uiso 1 1 calc R U . . . C38 C 0.9108(3) 0.70668(15) 0.5668(3) 0.0241(8) Uani 1 1 d . . . . . H38 H 0.850291 0.730911 0.552142 0.029 Uiso 1 1 calc R U . . . C19 C 0.2624(3) 0.68039(14) 0.3841(3) 0.0213(8) Uani 1 1 d . . . . . C43 C 0.3937(3) 0.88722(16) 0.6433(3) 0.0284(9) Uani 1 1 d . . . . . H43 H 0.331129 0.907050 0.653241 0.034 Uiso 1 1 calc R U . . . C18 C 0.2179(3) 0.73214(15) 0.3653(3) 0.0245(9) Uani 1 1 d . . . . . H18 H 0.149979 0.741862 0.316275 0.029 Uiso 1 1 calc R U . . . C40 C 0.5754(3) 0.83010(14) 0.6123(3) 0.0225(8) Uani 1 1 d . . . . . H40 H 0.638159 0.810795 0.601275 0.027 Uiso 1 1 calc R U . . . C41 C 0.5866(3) 0.88295(15) 0.6336(3) 0.0256(9) Uani 1 1 d . . . . . H41 H 0.657350 0.899558 0.638916 0.031 Uiso 1 1 calc R U . . . C24 C -0.1186(3) 0.64318(16) 0.1311(3) 0.0295(9) Uani 1 1 d . . . . . H24 H -0.190701 0.645239 0.083208 0.035 Uiso 1 1 calc R U . . . C5 C 0.5086(3) 0.51177(14) 0.3612(3) 0.0212(8) Uani 1 1 d . . . . . C37 C 1.0207(3) 0.72440(15) 0.5794(3) 0.0266(9) Uani 1 1 d . . . . . H37 H 1.034976 0.760485 0.573605 0.032 Uiso 1 1 calc R U . . . C33 C 0.8876(3) 0.65396(15) 0.5754(3) 0.0218(8) Uani 1 1 d . . . . . C17 C 0.2899(3) 0.76419(15) 0.4298(3) 0.0219(8) Uani 1 1 d . . . . . H17 H 0.282620 0.800866 0.434275 0.026 Uiso 1 1 calc R U . . . C45 C 0.8281(3) 0.67982(16) 0.8042(3) 0.0298(10) Uani 1 1 d . . . . . C36 C 1.1093(3) 0.68946(15) 0.6002(3) 0.0276(9) Uani 1 1 d . . . . . H36 H 1.184512 0.701520 0.608704 0.033 Uiso 1 1 calc R U . . . C44 C 0.3820(3) 0.83400(15) 0.6252(3) 0.0248(9) Uani 1 1 d . . . . . H44 H 0.312456 0.817317 0.625233 0.030 Uiso 1 1 calc R U . . . C20 C 0.2082(3) 0.63464(15) 0.3435(3) 0.0226(8) Uani 1 1 d . . . . . C29 C 0.4553(3) 0.40629(16) 0.1502(3) 0.0316(10) Uani 1 1 d . . . . . H29 H 0.406213 0.400443 0.082246 0.038 Uiso 1 1 calc R U . . . C22 C 0.0021(3) 0.65916(15) 0.3048(3) 0.0267(9) Uani 1 1 d . . . . . H22 H 0.012062 0.672170 0.375565 0.032 Uiso 1 1 calc R U . . . C42 C 0.4950(3) 0.91134(15) 0.6469(3) 0.0281(9) Uani 1 1 d . . . . . H42 H 0.501919 0.947789 0.658739 0.034 Uiso 1 1 calc R U . . . C31 C 0.6051(3) 0.37830(15) 0.2921(4) 0.0316(10) Uani 1 1 d . . . . . H31 H 0.659178 0.352740 0.323025 0.038 Uiso 1 1 calc R U . . . C32 C 0.5971(3) 0.42431(15) 0.3482(3) 0.0259(9) Uani 1 1 d . . . . . H32 H 0.646907 0.430031 0.415917 0.031 Uiso 1 1 calc R U . . . C35 C 1.0883(3) 0.63683(16) 0.6087(3) 0.0299(9) Uani 1 1 d . . . . . H35 H 1.149321 0.612866 0.623042 0.036 Uiso 1 1 calc R U . . . C30 C 0.5357(3) 0.36965(16) 0.1930(4) 0.0337(10) Uani 1 1 d . . . . . H30 H 0.543022 0.338807 0.154515 0.040 Uiso 1 1 calc R U . . . C34 C 0.9783(3) 0.61898(16) 0.5963(3) 0.0290(9) Uani 1 1 d . . . . . H34 H 0.964510 0.582843 0.602097 0.035 Uiso 1 1 calc R U . . . C47 C -0.1781(4) 0.47659(19) 0.0856(4) 0.0415(11) Uani 1 1 d . . . . . H47 H -0.129238 0.497269 0.144435 0.050 Uiso 1 1 calc R U . . . F1 F 0.8652(6) 0.6327(3) 0.7992(6) 0.0311(17) Uani 0.4 1 d . U P A 2 F7 F 0.8649(4) 0.71922(18) 0.8630(4) 0.0442(11) Uani 0.6 1 d . U P A 1 F8 F 0.7898(4) 0.64473(18) 0.8751(4) 0.0460(11) Uani 0.6 1 d . U P A 1 F3 F 0.9203(4) 0.7129(2) 0.7920(4) 0.0304(13) Uani 0.4 1 d . . P A 2 F2 F 0.8203(5) 0.6904(3) 0.8994(4) 0.0323(14) Uani 0.4 1 d . . P A 2 F9 F 0.9092(4) 0.6525(2) 0.7820(3) 0.0490(14) Uani 0.6 1 d . . P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0114(2) 0.0243(3) 0.0185(3) -0.0042(2) 0.00076(19) 0.00084(19) Cl2 0.0315(5) 0.0430(6) 0.0395(6) -0.0045(5) 0.0064(5) -0.0046(5) Cl1 0.0339(6) 0.0603(8) 0.0456(7) -0.0100(6) 0.0115(5) 0.0061(5) Cl3 0.0490(7) 0.0515(7) 0.0518(8) 0.0044(6) 0.0025(6) 0.0137(6) F6 0.0463(15) 0.0378(14) 0.0414(15) -0.0204(12) 0.0224(12) -0.0212(12) F5 0.0225(12) 0.0635(17) 0.0249(13) -0.0090(12) 0.0069(10) 0.0092(11) F4 0.0576(16) 0.0363(14) 0.0199(13) 0.0003(11) 0.0053(11) 0.0058(12) N3 0.0137(14) 0.0229(16) 0.0182(16) -0.0014(13) 0.0013(12) 0.0009(12) N4 0.0130(14) 0.0255(17) 0.0191(17) -0.0020(13) 0.0015(12) -0.0010(12) O2 0.0296(16) 0.0375(17) 0.0460(19) -0.0033(15) 0.0014(14) -0.0088(13) N2 0.0137(14) 0.0264(17) 0.0181(16) -0.0030(13) 0.0005(12) -0.0013(12) O1 0.0283(16) 0.0495(19) 0.056(2) -0.0008(16) 0.0219(15) 0.0010(14) N1 0.0153(15) 0.0249(17) 0.0212(17) -0.0035(13) 0.0012(13) 0.0022(12) N00E 0.0235(18) 0.033(2) 0.034(2) 0.0007(17) 0.0038(16) -0.0011(15) C14 0.0148(17) 0.0229(19) 0.018(2) 0.0003(15) 0.0033(15) -0.0031(14) C16 0.0148(17) 0.023(2) 0.019(2) -0.0021(16) 0.0040(15) 0.0000(14) C11 0.0146(17) 0.026(2) 0.019(2) 0.0005(16) 0.0007(15) 0.0003(15) C9 0.0149(17) 0.028(2) 0.017(2) 0.0025(16) 0.0012(15) 0.0028(15) C3 0.0193(19) 0.024(2) 0.024(2) -0.0032(16) 0.0057(16) -0.0016(15) C8 0.0151(18) 0.030(2) 0.024(2) -0.0008(17) 0.0035(16) 0.0033(15) C13 0.0189(18) 0.0229(19) 0.021(2) -0.0009(16) 0.0041(15) -0.0024(15) C46 0.0173(18) 0.026(2) 0.024(2) -0.0031(17) 0.0026(16) -0.0038(15) C4 0.0146(17) 0.025(2) 0.0185(19) -0.0005(16) 0.0026(14) 0.0001(15) C6 0.0192(18) 0.026(2) 0.0158(19) -0.0013(16) 0.0010(15) 0.0027(15) C25 0.0199(19) 0.034(2) 0.028(2) -0.0082(18) -0.0005(17) 0.0023(17) C15 0.0177(17) 0.025(2) 0.018(2) -0.0012(16) 0.0057(15) -0.0038(15) C12 0.0173(18) 0.029(2) 0.020(2) -0.0019(17) 0.0003(15) -0.0038(15) C21 0.0151(18) 0.025(2) 0.027(2) -0.0055(17) 0.0006(16) 0.0017(15) C26 0.0159(18) 0.031(2) 0.030(2) -0.0086(18) 0.0042(16) 0.0024(16) C7 0.0197(18) 0.025(2) 0.023(2) -0.0022(17) 0.0046(16) 0.0037(16) C2 0.0147(18) 0.034(2) 0.024(2) -0.0064(18) 0.0025(16) -0.0015(16) C28 0.0212(19) 0.026(2) 0.030(2) -0.0022(18) 0.0061(17) 0.0014(16) C10 0.0163(18) 0.028(2) 0.018(2) -0.0009(16) -0.0017(15) 0.0022(15) C39 0.0210(19) 0.024(2) 0.021(2) -0.0016(16) 0.0046(16) -0.0008(15) C1 0.0126(17) 0.031(2) 0.022(2) -0.0073(17) 0.0013(15) -0.0011(15) C27 0.0188(18) 0.0226(19) 0.024(2) 0.0001(16) 0.0066(16) -0.0009(15) C23 0.0141(18) 0.040(2) 0.036(3) -0.002(2) 0.0031(17) 0.0057(17) C38 0.0183(18) 0.027(2) 0.025(2) -0.0010(17) 0.0011(16) 0.0039(16) C19 0.0114(16) 0.030(2) 0.022(2) -0.0040(16) 0.0021(15) 0.0014(15) C43 0.023(2) 0.032(2) 0.029(2) -0.0052(18) 0.0026(17) 0.0062(17) C18 0.0175(18) 0.032(2) 0.021(2) -0.0003(17) 0.0004(16) 0.0035(16) C40 0.0205(19) 0.025(2) 0.021(2) -0.0016(16) 0.0042(16) -0.0012(15) C41 0.024(2) 0.026(2) 0.026(2) 0.0013(17) 0.0029(17) -0.0026(16) C24 0.0152(18) 0.036(2) 0.033(2) -0.0011(19) -0.0029(17) 0.0029(16) C5 0.0200(18) 0.027(2) 0.0162(19) 0.0018(16) 0.0033(15) 0.0021(15) C37 0.023(2) 0.024(2) 0.030(2) -0.0006(17) 0.0012(17) -0.0026(16) C33 0.0151(18) 0.029(2) 0.020(2) -0.0048(16) 0.0008(15) 0.0008(15) C17 0.0170(18) 0.024(2) 0.024(2) -0.0007(16) 0.0035(16) -0.0001(15) C45 0.026(2) 0.036(2) 0.024(2) -0.0096(19) -0.0027(17) 0.0075(18) C36 0.0154(18) 0.035(2) 0.031(2) 0.0014(18) 0.0023(16) -0.0030(16) C44 0.0175(18) 0.032(2) 0.025(2) -0.0023(17) 0.0043(16) 0.0005(16) C20 0.0125(17) 0.032(2) 0.022(2) -0.0066(17) 0.0014(15) 0.0012(15) C29 0.028(2) 0.034(2) 0.033(2) -0.0076(19) 0.0067(18) -0.0081(18) C22 0.0185(19) 0.032(2) 0.028(2) -0.0095(18) 0.0036(16) 0.0008(16) C42 0.031(2) 0.025(2) 0.027(2) -0.0035(18) 0.0028(18) 0.0016(17) C31 0.023(2) 0.020(2) 0.056(3) 0.0091(19) 0.018(2) 0.0036(16) C32 0.0175(18) 0.032(2) 0.028(2) 0.0067(18) 0.0055(16) -0.0018(16) C35 0.0163(19) 0.031(2) 0.040(3) 0.0042(19) 0.0019(17) 0.0046(16) C30 0.031(2) 0.026(2) 0.047(3) -0.010(2) 0.016(2) -0.0088(18) C34 0.0178(19) 0.026(2) 0.041(3) 0.0007(18) 0.0025(18) -0.0022(16) C47 0.036(2) 0.052(3) 0.034(3) -0.007(2) 0.002(2) 0.002(2) F1 0.030(2) 0.030(2) 0.032(2) 0.0003(17) 0.0033(17) 0.0027(17) F7 0.0407(17) 0.0465(18) 0.0410(18) -0.0053(16) 0.0008(15) -0.0015(15) F8 0.0425(17) 0.0500(18) 0.0435(18) 0.0059(15) 0.0061(14) 0.0005(15) F3 0.015(3) 0.039(3) 0.028(3) -0.001(3) -0.014(2) -0.010(2) F2 0.033(3) 0.050(4) 0.010(3) -0.002(3) -0.003(2) 0.020(3) F9 0.030(3) 0.089(4) 0.022(2) -0.006(3) -0.005(2) 0.031(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N4 Co1 N3 90.23(12) . . ? N2 Co1 N3 90.17(12) . . ? N2 Co1 N4 171.18(13) . . ? N1 Co1 N3 171.24(13) . . ? N1 Co1 N4 90.52(12) . . ? N1 Co1 N2 90.42(12) . . ? C14 N3 Co1 124.6(2) . . ? C11 N3 Co1 125.8(2) . . ? C11 N3 C14 106.9(3) . . ? C16 N4 Co1 125.1(2) . . ? C19 N4 Co1 125.5(2) . . ? C19 N4 C16 105.6(3) . . ? C9 N2 Co1 124.3(2) . . ? C6 N2 Co1 127.1(2) . . ? C6 N2 C9 105.5(3) . . ? C4 N1 Co1 126.4(2) . . ? C1 N1 Co1 126.1(2) . . ? C1 N1 C4 106.3(3) . . ? O2 N00E C2 117.1(3) . . ? O1 N00E O2 124.6(3) . . ? O1 N00E C2 118.2(3) . . ? N3 C14 C13 109.0(3) . . ? N3 C14 C15 121.0(3) . . ? C15 C14 C13 128.6(3) . . ? N4 C16 C17 109.2(3) . . ? C15 C16 N4 123.6(3) . . ? C15 C16 C17 127.0(3) . . ? N3 C11 C12 109.0(3) . . ? N3 C11 C10 121.1(3) . . ? C10 C11 C12 129.2(3) . . ? N2 C9 C8 109.7(3) . . ? C10 C9 N2 124.0(3) . . ? C10 C9 C8 125.8(3) . . ? C4 C3 H3 127.1 . . ? C2 C3 H3 127.1 . . ? C2 C3 C4 105.9(3) . . ? C9 C8 H8 126.6 . . ? C7 C8 C9 106.8(3) . . ? C7 C8 H8 126.6 . . ? C14 C13 C46 125.5(3) . . ? C12 C13 C14 106.7(3) . . ? C12 C13 C46 127.1(3) . . ? F6 C46 C13 113.0(3) . . ? F5 C46 F6 106.8(3) . . ? F5 C46 F4 105.5(3) . . ? F5 C46 C13 112.9(3) . . ? F4 C46 F6 105.4(3) . . ? F4 C46 C13 112.5(3) . . ? N1 C4 C3 110.2(3) . . ? N1 C4 C5 124.1(3) . . ? C5 C4 C3 125.1(3) . . ? N2 C6 C7 110.0(3) . . ? N2 C6 C5 124.2(3) . . ? C5 C6 C7 125.8(3) . . ? C26 C25 H25 120.1 . . ? C24 C25 H25 120.1 . . ? C24 C25 C26 119.8(4) . . ? C14 C15 C39 118.5(3) . . ? C16 C15 C14 121.1(3) . . ? C16 C15 C39 119.4(3) . . ? C11 C12 C45 126.0(3) . . ? C13 C12 C11 107.1(3) . . ? C13 C12 C45 126.0(3) . . ? C26 C21 C20 119.2(3) . . ? C26 C21 C22 119.0(3) . . ? C22 C21 C20 121.9(3) . . ? C25 C26 C21 121.0(3) . . ? C25 C26 H26 119.5 . . ? C21 C26 H26 119.5 . . ? C8 C7 C6 107.6(3) . . ? C8 C7 H7 126.2 . . ? C6 C7 H7 126.2 . . ? C3 C2 N00E 122.6(4) . . ? C3 C2 C1 109.7(3) . . ? C1 C2 N00E 127.4(3) . . ? C27 C28 H28 119.4 . . ? C29 C28 H28 119.4 . . ? C29 C28 C27 121.3(4) . . ? C11 C10 C33 118.6(3) . . ? C9 C10 C11 120.5(3) . . ? C9 C10 C33 120.2(3) . . ? C40 C39 C15 117.9(3) . . ? C40 C39 C44 118.8(3) . . ? C44 C39 C15 123.3(3) . . ? N1 C1 C2 107.5(3) . . ? N1 C1 C20 123.7(3) . . ? C20 C1 C2 128.0(3) . . ? C28 C27 C5 120.2(3) . . ? C32 C27 C28 117.8(3) . . ? C32 C27 C5 121.9(3) . . ? C24 C23 H23 119.7 . . ? C24 C23 C22 120.5(4) . . ? C22 C23 H23 119.7 . . ? C37 C38 H38 119.4 . . ? C37 C38 C33 121.1(3) . . ? C33 C38 H38 119.4 . . ? N4 C19 C18 109.9(3) . . ? N4 C19 C20 123.6(3) . . ? C20 C19 C18 126.3(3) . . ? C44 C43 H43 119.8 . . ? C42 C43 H43 119.8 . . ? C42 C43 C44 120.5(4) . . ? C19 C18 H18 126.4 . . ? C17 C18 C19 107.3(3) . . ? C17 C18 H18 126.4 . . ? C39 C40 H40 119.7 . . ? C41 C40 C39 120.6(3) . . ? C41 C40 H40 119.7 . . ? C40 C41 H41 120.1 . . ? C42 C41 C40 119.8(4) . . ? C42 C41 H41 120.1 . . ? C25 C24 H24 120.0 . . ? C23 C24 C25 120.0(4) . . ? C23 C24 H24 120.0 . . ? C4 C5 C27 119.0(3) . . ? C6 C5 C4 121.4(3) . . ? C6 C5 C27 119.3(3) . . ? C38 C37 H37 120.0 . . ? C36 C37 C38 119.9(4) . . ? C36 C37 H37 120.0 . . ? C38 C33 C10 118.3(3) . . ? C38 C33 C34 118.3(3) . . ? C34 C33 C10 123.4(3) . . ? C16 C17 H17 126.2 . . ? C18 C17 C16 107.7(3) . . ? C18 C17 H17 126.2 . . ? F1 C45 C12 112.1(4) . . ? F1 C45 F3 104.7(5) . . ? F7 C45 C12 114.1(4) . . ? F7 C45 F8 104.1(4) . . ? F7 C45 F9 112.2(4) . . ? F8 C45 C12 106.2(3) . . ? F3 C45 C12 108.7(4) . . ? F2 C45 C12 117.4(4) . . ? F2 C45 F1 110.5(5) . . ? F2 C45 F3 102.2(5) . . ? F9 C45 C12 117.9(4) . . ? F9 C45 F8 100.2(4) . . ? C37 C36 H36 120.0 . . ? C37 C36 C35 120.0(3) . . ? C35 C36 H36 120.0 . . ? C39 C44 H44 120.1 . . ? C43 C44 C39 119.8(3) . . ? C43 C44 H44 120.1 . . ? C1 C20 C21 119.2(3) . . ? C19 C20 C21 119.1(3) . . ? C19 C20 C1 121.4(3) . . ? C28 C29 H29 119.8 . . ? C30 C29 C28 120.4(4) . . ? C30 C29 H29 119.8 . . ? C21 C22 C23 119.7(4) . . ? C21 C22 H22 120.1 . . ? C23 C22 H22 120.1 . . ? C43 C42 C41 120.4(4) . . ? C43 C42 H42 119.8 . . ? C41 C42 H42 119.8 . . ? C32 C31 H31 119.6 . . ? C30 C31 H31 119.6 . . ? C30 C31 C32 120.9(4) . . ? C27 C32 C31 120.4(4) . . ? C27 C32 H32 119.8 . . ? C31 C32 H32 119.8 . . ? C36 C35 H35 119.9 . . ? C36 C35 C34 120.2(4) . . ? C34 C35 H35 119.9 . . ? C29 C30 H30 120.4 . . ? C31 C30 C29 119.1(4) . . ? C31 C30 H30 120.4 . . ? C33 C34 H34 119.8 . . ? C35 C34 C33 120.4(4) . . ? C35 C34 H34 119.8 . . ? Cl2 C47 H47 108.9 . . ? Cl1 C47 Cl2 110.2(2) . . ? Cl1 C47 Cl3 109.1(3) . . ? Cl1 C47 H47 108.9 . . ? Cl3 C47 Cl2 110.8(3) . . ? Cl3 C47 H47 108.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N3 1.942(3) . ? Co1 N4 1.938(3) . ? Co1 N2 1.935(3) . ? Co1 N1 1.927(3) . ? Cl2 C47 1.763(5) . ? Cl1 C47 1.760(5) . ? Cl3 C47 1.761(5) . ? F6 C46 1.337(4) . ? F5 C46 1.330(4) . ? F4 C46 1.330(4) . ? N3 C14 1.377(5) . ? N3 C11 1.376(4) . ? N4 C16 1.389(5) . ? N4 C19 1.379(4) . ? O2 N00E 1.229(4) . ? N2 C9 1.391(4) . ? N2 C6 1.375(5) . ? O1 N00E 1.225(4) . ? N1 C4 1.387(5) . ? N1 C1 1.386(4) . ? N00E C2 1.454(5) . ? C14 C13 1.437(5) . ? C14 C15 1.413(5) . ? C16 C15 1.382(5) . ? C16 C17 1.438(5) . ? C11 C12 1.434(5) . ? C11 C10 1.411(5) . ? C9 C8 1.443(5) . ? C9 C10 1.387(5) . ? C3 H3 0.9500 . ? C3 C4 1.433(5) . ? C3 C2 1.341(5) . ? C8 H8 0.9500 . ? C8 C7 1.347(5) . ? C13 C46 1.499(5) . ? C13 C12 1.377(5) . ? C4 C5 1.395(5) . ? C6 C7 1.440(5) . ? C6 C5 1.394(5) . ? C25 H25 0.9500 . ? C25 C26 1.385(5) . ? C25 C24 1.379(5) . ? C15 C39 1.488(5) . ? C12 C45 1.499(5) . ? C21 C26 1.388(5) . ? C21 C20 1.496(5) . ? C21 C22 1.393(5) . ? C26 H26 0.9500 . ? C7 H7 0.9500 . ? C2 C1 1.442(5) . ? C28 H28 0.9500 . ? C28 C27 1.396(5) . ? C28 C29 1.386(6) . ? C10 C33 1.489(5) . ? C39 C40 1.393(5) . ? C39 C44 1.399(5) . ? C1 C20 1.394(5) . ? C27 C5 1.490(5) . ? C27 C32 1.387(5) . ? C23 H23 0.9500 . ? C23 C24 1.379(6) . ? C23 C22 1.394(5) . ? C38 H38 0.9500 . ? C38 C37 1.388(5) . ? C38 C33 1.394(5) . ? C19 C18 1.436(5) . ? C19 C20 1.390(5) . ? C43 H43 0.9500 . ? C43 C44 1.390(6) . ? C43 C42 1.372(6) . ? C18 H18 0.9500 . ? C18 C17 1.341(5) . ? C40 H40 0.9500 . ? C40 C41 1.386(5) . ? C41 H41 0.9500 . ? C41 C42 1.378(5) . ? C24 H24 0.9500 . ? C37 H37 0.9500 . ? C37 C36 1.382(5) . ? C33 C34 1.401(5) . ? C17 H17 0.9500 . ? C45 F1 1.300(8) . ? C45 F7 1.281(6) . ? C45 F8 1.435(6) . ? C45 F3 1.446(7) . ? C45 F2 1.279(7) . ? C45 F9 1.297(6) . ? C36 H36 0.9500 . ? C36 C35 1.386(6) . ? C44 H44 0.9500 . ? C29 H29 0.9500 . ? C29 C30 1.378(6) . ? C22 H22 0.9500 . ? C42 H42 0.9500 . ? C31 H31 0.9500 . ? C31 C32 1.400(6) . ? C31 C30 1.374(6) . ? C32 H32 0.9500 . ? C35 H35 0.9500 . ? C35 C34 1.391(5) . ? C30 H30 0.9500 . ? C34 H34 0.9500 . ? C47 H47 1.0000 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N3 C14 C13 150.8(2) . . . . ? Co1 N3 C14 C15 -41.6(4) . . . . ? Co1 N3 C11 C12 -151.5(3) . . . . ? Co1 N3 C11 C10 36.9(5) . . . . ? Co1 N4 C16 C15 -31.7(5) . . . . ? Co1 N4 C16 C17 153.1(2) . . . . ? Co1 N4 C19 C18 -153.4(3) . . . . ? Co1 N4 C19 C20 31.4(5) . . . . ? Co1 N2 C9 C8 -154.9(2) . . . . ? Co1 N2 C9 C10 33.3(5) . . . . ? Co1 N2 C6 C7 155.9(3) . . . . ? Co1 N2 C6 C5 -24.0(5) . . . . ? Co1 N1 C4 C3 161.9(3) . . . . ? Co1 N1 C4 C5 -26.7(5) . . . . ? Co1 N1 C1 C2 -161.5(3) . . . . ? Co1 N1 C1 C20 28.2(5) . . . . ? N3 C14 C13 C46 -162.9(3) . . . . ? N3 C14 C13 C12 8.2(4) . . . . ? N3 C14 C15 C16 26.2(5) . . . . ? N3 C14 C15 C39 -142.6(3) . . . . ? N3 C11 C12 C13 -5.5(4) . . . . ? N3 C11 C12 C45 164.2(4) . . . . ? N3 C11 C10 C9 -30.4(5) . . . . ? N3 C11 C10 C33 140.7(4) . . . . ? N4 C16 C15 C14 11.4(5) . . . . ? N4 C16 C15 C39 -179.9(3) . . . . ? N4 C16 C17 C18 4.1(4) . . . . ? N4 C19 C18 C17 -3.1(4) . . . . ? N4 C19 C20 C21 175.5(3) . . . . ? N4 C19 C20 C1 -11.4(6) . . . . ? O2 N00E C2 C3 -41.0(5) . . . . ? O2 N00E C2 C1 146.1(4) . . . . ? N2 C9 C8 C7 -5.7(4) . . . . ? N2 C9 C10 C11 -5.6(6) . . . . ? N2 C9 C10 C33 -176.4(3) . . . . ? N2 C6 C7 C8 1.1(4) . . . . ? N2 C6 C5 C4 13.5(6) . . . . ? N2 C6 C5 C27 -173.5(3) . . . . ? O1 N00E C2 C3 136.6(4) . . . . ? O1 N00E C2 C1 -36.2(6) . . . . ? N1 C4 C5 C6 12.4(6) . . . . ? N1 C4 C5 C27 -160.6(3) . . . . ? N1 C1 C20 C21 153.8(4) . . . . ? N1 C1 C20 C19 -19.2(6) . . . . ? N00E C2 C1 N1 168.7(4) . . . . ? N00E C2 C1 C20 -21.6(7) . . . . ? C14 N3 C11 C12 10.5(4) . . . . ? C14 N3 C11 C10 -161.1(3) . . . . ? C14 C13 C46 F6 -115.8(4) . . . . ? C14 C13 C46 F5 5.6(5) . . . . ? C14 C13 C46 F4 125.0(4) . . . . ? C14 C13 C12 C11 -1.6(4) . . . . ? C14 C13 C12 C45 -171.3(4) . . . . ? C14 C15 C39 C40 44.2(5) . . . . ? C14 C15 C39 C44 -138.9(4) . . . . ? C16 N4 C19 C18 5.5(4) . . . . ? C16 N4 C19 C20 -169.7(3) . . . . ? C16 C15 C39 C40 -124.8(4) . . . . ? C16 C15 C39 C44 52.1(5) . . . . ? C11 N3 C14 C13 -11.5(4) . . . . ? C11 N3 C14 C15 156.1(3) . . . . ? C11 C12 C45 F1 -23.0(7) . . . . ? C11 C12 C45 F7 151.4(4) . . . . ? C11 C12 C45 F8 -94.5(5) . . . . ? C11 C12 C45 F3 92.3(5) . . . . ? C11 C12 C45 F2 -152.5(5) . . . . ? C11 C12 C45 F9 16.7(7) . . . . ? C11 C10 C33 C38 -48.5(5) . . . . ? C11 C10 C33 C34 132.9(4) . . . . ? C9 N2 C6 C7 -4.5(4) . . . . ? C9 N2 C6 C5 175.6(3) . . . . ? C9 C8 C7 C6 2.7(4) . . . . ? C9 C10 C33 C38 122.6(4) . . . . ? C9 C10 C33 C34 -56.1(5) . . . . ? C3 C4 C5 C6 -177.6(3) . . . . ? C3 C4 C5 C27 9.4(6) . . . . ? C3 C2 C1 N1 -5.0(4) . . . . ? C3 C2 C1 C20 164.8(4) . . . . ? C8 C9 C10 C11 -176.1(4) . . . . ? C8 C9 C10 C33 13.1(6) . . . . ? C13 C14 C15 C16 -168.9(4) . . . . ? C13 C14 C15 C39 22.3(5) . . . . ? C13 C12 C45 F1 144.8(5) . . . . ? C13 C12 C45 F7 -40.8(6) . . . . ? C13 C12 C45 F8 73.3(5) . . . . ? C13 C12 C45 F3 -99.9(5) . . . . ? C13 C12 C45 F2 15.3(7) . . . . ? C13 C12 C45 F9 -175.5(5) . . . . ? C46 C13 C12 C11 169.3(3) . . . . ? C46 C13 C12 C45 -0.4(6) . . . . ? C4 N1 C1 C2 6.6(4) . . . . ? C4 N1 C1 C20 -163.7(4) . . . . ? C4 C3 C2 N00E -172.8(3) . . . . ? C4 C3 C2 C1 1.2(4) . . . . ? C6 N2 C9 C8 6.2(4) . . . . ? C6 N2 C9 C10 -165.6(3) . . . . ? C15 C14 C13 C46 30.6(6) . . . . ? C15 C14 C13 C12 -158.2(4) . . . . ? C15 C16 C17 C18 -170.9(4) . . . . ? C15 C39 C40 C41 175.9(3) . . . . ? C15 C39 C44 C43 -173.9(4) . . . . ? C12 C11 C10 C9 159.9(4) . . . . ? C12 C11 C10 C33 -29.1(6) . . . . ? C12 C13 C46 F6 74.9(5) . . . . ? C12 C13 C46 F5 -163.7(4) . . . . ? C12 C13 C46 F4 -44.3(5) . . . . ? C26 C25 C24 C23 0.1(6) . . . . ? C26 C21 C20 C1 -54.2(5) . . . . ? C26 C21 C20 C19 119.0(4) . . . . ? C26 C21 C22 C23 -0.1(6) . . . . ? C7 C6 C5 C4 -166.4(4) . . . . ? C7 C6 C5 C27 6.6(6) . . . . ? C2 C3 C4 N1 3.1(4) . . . . ? C2 C3 C4 C5 -168.2(4) . . . . ? C2 C1 C20 C21 -14.4(6) . . . . ? C2 C1 C20 C19 172.5(4) . . . . ? C28 C27 C5 C4 46.3(5) . . . . ? C28 C27 C5 C6 -126.9(4) . . . . ? C28 C27 C32 C31 -0.2(5) . . . . ? C28 C29 C30 C31 0.9(6) . . . . ? C10 C11 C12 C13 165.3(4) . . . . ? C10 C11 C12 C45 -25.1(6) . . . . ? C10 C9 C8 C7 165.9(4) . . . . ? C10 C33 C34 C35 179.0(4) . . . . ? C39 C40 C41 C42 -1.6(6) . . . . ? C1 N1 C4 C3 -6.1(4) . . . . ? C1 N1 C4 C5 165.3(4) . . . . ? C27 C28 C29 C30 0.4(6) . . . . ? C38 C37 C36 C35 -0.1(6) . . . . ? C38 C33 C34 C35 0.4(6) . . . . ? C19 N4 C16 C15 169.3(3) . . . . ? C19 N4 C16 C17 -5.9(4) . . . . ? C19 C18 C17 C16 -0.6(4) . . . . ? C18 C19 C20 C21 1.1(6) . . . . ? C18 C19 C20 C1 174.2(4) . . . . ? C40 C39 C44 C43 3.0(6) . . . . ? C40 C41 C42 C43 2.5(6) . . . . ? C24 C25 C26 C21 -0.8(6) . . . . ? C24 C23 C22 C21 -0.5(6) . . . . ? C5 C6 C7 C8 -179.0(4) . . . . ? C5 C27 C32 C31 -177.8(3) . . . . ? C37 C38 C33 C10 -179.1(3) . . . . ? C37 C38 C33 C34 -0.5(6) . . . . ? C37 C36 C35 C34 0.0(6) . . . . ? C33 C38 C37 C36 0.3(6) . . . . ? C17 C16 C15 C14 -174.3(3) . . . . ? C17 C16 C15 C39 -5.6(6) . . . . ? C36 C35 C34 C33 -0.1(6) . . . . ? C44 C39 C40 C41 -1.1(6) . . . . ? C44 C43 C42 C41 -0.6(6) . . . . ? C20 C21 C26 C25 -178.6(4) . . . . ? C20 C21 C22 C23 179.2(4) . . . . ? C20 C19 C18 C17 171.9(4) . . . . ? C29 C28 C27 C5 177.0(3) . . . . ? C29 C28 C27 C32 -0.7(6) . . . . ? C22 C21 C26 C25 0.8(6) . . . . ? C22 C21 C20 C1 126.4(4) . . . . ? C22 C21 C20 C19 -60.3(5) . . . . ? C22 C23 C24 C25 0.5(6) . . . . ? C42 C43 C44 C39 -2.2(6) . . . . ? C32 C27 C5 C4 -136.1(4) . . . . ? C32 C27 C5 C6 50.7(5) . . . . ? C32 C31 C30 C29 -1.8(6) . . . . ? C30 C31 C32 C27 1.5(6) . . . . ?